Gas chromatography-mass spectrometry analysis of environmental sample AE04589 conducted April 4, 2002, detecting unknown compounds and surrogates.
NYC-WTC_000058231–000058238Folder label: “GCMS X 3/2/02 A 3/27/02”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document
Quantitation Report (QT Reviewed)
Data File ; C:\HPCHEM\1\DATA\MAR27O2\4589.D Vial: 12 Acq On : 28 Mar 2002 12:33 am Operator: Sample : gc/ms scan 3/2 Inst ; GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: Mar 29 12:49 2002 Quant Results File; GCMS0308.RES
Quant Method : C:\HPCHEM\1\METHODS\GCMS0308.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Fri Mar 29 10:31:28 2002 Response via : Initial Calibration DataAcq Meth : GCMS0308
Internal Standards R.T. Qlon Response Cone Units Dev(Min)
1) 1,4-Dichlorobenzene-d4 12.25 152 749305 20.00 ug/1 -0.10 10) Naphthalene-d8 15.89 136 2920472 20.00 ug/1 -0.11 17) Acenaphthene-dlO 21.20 164 1599258 20.00 ug/1 -0.12 29) Phenanthrene-dlO 25.64 188 2322297 20.00 ug/1 -0.13 38) Chrysene-dl2 33.70 240 1263379 20.00 ug/1 -0.15 44) Perylene-dl2 37.95 264 748619 20.00 ug/1 -0.17
System Monitoring Compounds 37) 2,4-DDD 30.72 235 90589 3.89 ug/mL 0.22 Spiked Amount 5.000 Recovery = 77.80%
Target Compounds Qvalue 2) N-nitroso-dimethyl amine 0.00 74 0 N.D. 3) bis(2-Chloroethyl)ether 0.00 93 0 N.D. 4) 1,3-Dichlorobenzene 12.30 146 590 N.D. 5) 1,4-Dichlorobenzene 12.30 146 590 ■ N.D. 6) 1,2-Dichlorobenzene 0.00 146 0 N.D. 7) 2,2'-oxybi s(1-Chioropropan 0.00 45 0 N.D. 8) N-Nitroso-di-n-propylamine 0.00 70 0 N.D. 9) Hexachioroethane 0.00 117 0 N.D. 11) Nitrobenzene 0.00 77 0 N.D. 12) Isophorone 0.00 82 0 N.D. 13) bis(2-Chloroethoxy)methane 0.00 93 0 N.D. 14) 1,2,4-Trichlorobenzene 0.00 180 0 N.D. 15) Naphthalene 15.94 128 604 N.D. 16) Hexachlorobutadiene 0.00 225 0 N.D. 18) Hexachlorocyclopentadiene 0.00 237 0 N.D. 19) 2-Chloronaphthalene 0.00 162 0 N.D. 20) Dimethylphthalate 0.00 163 0 N.D. 21) 2,6-Dinitrotoluene 0.00 165 0 N.D. 22) Acenaphthylene 0.00 152 0 N.D. 2 3) Acenaphthene 0.00 153 0 N.D. 24) 2,4-Dinitrotoluene 21.58 165 179 N.D. 25) Diethylphthalate 22.67 149 939 N.D. 26) 4-Chlorophenyl-phenylether 0.00 204 0 N.D. 27) Fluorene 0.00 166 0 N.D. 28) Azobenzen/ 1,2-Diphenylhyd 0.00 77 0 N.D.
(#) = qualifier out of range (m) = manual integration 4589.D GCMS0308.M Fri Mar 29 12:51:06 2002 Page 1
NYC-WTC_000058233
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NYC-WTC_000058199
GCMS analysis of sample AE04517 for organic compounds with surrogate standard showing 84% recovery on April 4, 2002.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000058223
Gas chromatography-mass spectrometry analysis of environmental sample AE04588 conducted April 4, 2002, detecting unknown compounds and surrogates.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000058215
Gas chromatography-mass spectrometry analysis of environmental sample AE04519 conducted April 4, 2002, detecting unknown compounds and surrogates.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000058207
GCMS analysis of sample AE04518 for organic compounds with surrogate standard showing 70% recovery on April 4, 2002.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000058537
Laboratory report documenting GCMS analysis of sample AE04806 conducted on April 5, 2002.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000059737
Laboratory report detailing GCMS analysis of environmental sample AE05895 conducted on March 29, 2002.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000058283
Gas chromatography-mass spectrometry analysis of environmental sample AE04735 conducted April 4, 2002, detecting unknown compounds and surrogates.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000058580
Laboratory report documenting GCMS analysis of sample AE04847 conducted on April 5, 2002.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000058545
Laboratory report documenting GCMS analysis of sample AE04843 conducted on April 5, 2002.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000058299
Gas chromatography-mass spectrometry analysis of environmental sample AE04737 conducted April 4, 2002, detecting unknown compounds and surrogates.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000058838
Laboratory report page showing surrogate recovery data for sample AE05035 analyzed on April 5, 2002.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000058291
Gas chromatography-mass spectrometry analysis of environmental sample AE04736 conducted April 4, 2002, detecting unknown compounds and surrogates.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗No available related records indexed in this group.
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NYC-WTC_000058159
Unreadable text fragment containing a file identifier from the March 2002 GCMS batch records.
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NYC-WTC_000058160
Fragmented text containing a unique file identifier from the March 2002 GCMS batch records.
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NYC-WTC_000058163
Laboratory blank analysis report showing all target compounds detected below the method detection limit on March 29, 2002.
Filed in the same folder
NYC-WTC_000058171
Calibration log listing response factors for nitrosamines and chlorinated solvents on March 29, 2002.
Filed in the same folder
NYC-WTC_000058175
Analysis of reference standards for nitrosamines and VOCs with measured concentrations near target levels on March 29, 2002.
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