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GCMS sample analysis with surrogate recovery, Apr 2002

Machine-extracted title · confidence 100%

GCMS analysis of sample AE04516 for organic compounds with surrogate standard 2,4-DDD showing 75% recovery.

NYC-WTC_000058191–000058198

Folder label: “GCMS X 3/2/02 A 3/27/02

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NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed)

Data File : C:\HPCHEM\l\DATA\MAR2702\4516.D Vial: 7 Acq On : 27 Mar 2002 7:36 pm Operator: Sample : gc/ms scan 3/2 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: Mar 29 12:39 2002 Quant Results File: GCMS0308.RES

Quant Method : C:\HPCHEM\1\METHODS\GCMS0308.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Fri Mar 29 10:31:28 2002 Response via : Initial Calibration DataAcq Meth : GCMS0308

Compound R.T. Qlon Response Cone Unit Qvalue

30) N-Nitrosodiphenylamine 0.00 168 0 N.D. 31) 4-Bromophenyl-phenylether 0.00 248 0 N.D. 32) Hexachlorobenzene 0.00 284 0 N.D. 3 3) Phenanthrene 25.65 178 715 N.D. 34) Anthracene 25.65 178 715 N.D. 35) Di-n-butylphthalate 27.61 149 3079 N.D. 3 6) Fluoranthene 0.00 202 0 N.D. 39) Pyrene 0.00 202 0 N.D. 40) Butylbenzylphthalate 0.00 149 0 N.D. 41) Benzo(a)anthracene 33.70 228 3511 N.D. 42) Bis(2-ethylhexyl)phthalate 33.91 149 3014 N.D. 43) Chrysene 33.77 228 935 N.D. 45) Di-n-Octylphthalate 35.64 149 199 N.D. 46) Benzo(b)fluoranthene 36.77 252 974 N.D. 47) Benzo(k)fluoranthene 36.83 252 1233 N.D. 4 8) Benzo(a)pyrene 37.75 252 269 N.D. 4 9) Indeno(1,2,3-cd)pyrene 0.00 276 0 N.D. 50) Dibenz(a,h)anthracene 0.00 278 0 N.D. 51) Benzo(g,h,i)perylene 0.00 276 0 N.D.

(#) = qualifier out of range (m) = manual integration 4516.D GCMS0308.M Fri Mar 29 13:02:31 2002 Page 2

NYC-WTC_000058194

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NYC-WTC_000058194Source: NYC Law Department, mirrored locally

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