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GCMS sample analysis with surrogate recovery, Apr 2002

Machine-extracted title · confidence 100%

GCMS analysis of sample AE04416 for organic compounds with surrogate standard showing 5.0 micrograms detection limit.

NYC-WTC_000058183–000058190

Folder label: “GCMS X 3/2/02 A 3/27/02

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Scanned page image, NYC-WTC_000058188
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OCR status: ok · source: pdftotext

NYC 9/11 Public Portal Document

LSC Area Percent Report

‘Data File : C:\HPCHEM\l\DATA\MAR2702\4416 .D Vial: 6 Acq On : 27 Mar 2002 6:36 pm Operator: San^le : gc/ms scan 3/2 Inst : GC/MS 209 Mise Multiplr; 1.00 MS Integration Params: LSCINT.P

Method : C:\HPCHEM\1\METHODS\GCMS0308.M {RTE Integrator) Title : 209 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total

1 12.250 779 785 800 rBV 1903393 4528991 66.64% 14.605% 2 15.894 1175 1182 1199 rBV 2827611 6147371 90.45% 19.824% 3 21.201 1753 1760 1774 rBV 3195281 6796173 100.00% 21.916% 4 25.644 2236 2244 2255 rBV2 2965616 6356848 93.54% 20.499% 5 27.599 2452 2457 2465 rBV 87906 167433 2.46% 0.540%

6 30.711 2791 2796 2802 rBV 223806 440073 6.48% 1.419% 7 33.704 3111 3122 3141 rBV 1689521 3882834 57.13% 12.521% 8 37.946 3575 3584 3599 rBV2 866085 2690297 39.59% 8.676%

Sum of corrected areas: 31010020

4416.D GCMS0308.M Fri Mar 29 12:55:41 2002

NYC-WTC_000058188

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NYC-WTC_000058188Source: NYC Law Department, mirrored locally

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