Spiked sample analysis results for sample AD28318 showing pesticide compound responses on January 16, 2002.
NYC-WTC_000058049–000058052Folder label: “525 X 11/26/01 A 12/17 - 12/18/01”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document Quantitation Report (QT Reviewed)
Data File : C:\MSDCHEM\1\DATA\121701\28318S.D Vial: 38 Acq On : 18 Dec 2001 12:32 am Operator: McLean Sample : 1126 spk Inst : Instrumen Mise : Multiplr: 1.00 MS Integration Params: BENZO.P Quant Time: Dec 18 01:09:03 2001 Quant Results File: 121401.RES
Quant Method : C:\MSDCHEM\1\5973N\121401.M (RTE Integrator) Title : Quantitation For Method 525.2 Last Update : Mon Dec 17 15:06:05 2001 Response via : Initial Calibration DataAcq Meth : 121401
Internal Standards R.T. Qlon Response Cone Units Dev(Min)
1) Acenaphthene-diO 18.20 164 6024036 5.00 ug/L 0.00 9) Phenanthrene D-10 22.53 188 9440519 5.00 ug/L 0.00 20) Chrysene D-12 3 0.30 240 6505080 5.00 ug/L 0.00
System Monitoring Compounds 2) 1,3-Dimethyl -2 -nitrobenzen 13.13 134 1441985 4.68 ug/L 0.00 Spiked Amount 5.000 Recovery = 93.60% 19) Triphenyl Phosphate surr 29.58 326 1724900 6.00 ug/L 0.00 Spiked Amount 5.000 Recovery = 120.00% 21) Perylene D-12 surr 34.32 264 4733931 5.50 ug/L 0.00 Spiked Amount 5.000 Recovery = 110.00%
Target Compounds Qvalue 3) Hexachlorocyclopentadiene 15.71 237 631447 3.70 ug/L 97 4) Hexachlorobenzene 21.40 284 1666262 4.18 ug/L 97 5) EPTC 16.18 128 301.3567 5.25 ug/L 10 0 6) 2,6-Dinitrotoluene 17.77 165 1020271 3.64 ug/L 93 7) 2,4-Dinitotoluene 18.91 165 1258285 3.67 ug/L 94 8) Molinate 19.09 126 4617668 5.68 ug/L 95 10) Simazine 21.93 201 1303873 5.08 ug/L 98 11) Atrazine 22.05 200 2037871 6.08 ug/L 96 12) Alachlor 23.91 160 1871485 5.74 ug/L 94 13) Terbacil 22.88 161 2365899m 7.98 ug/L 14) Acetochlor 23.70 146 1327826 5.60 ug/L 96 15) Metribuzin 23.73 198 1339834 3.06 ug/L 99 16) Metolachlor 24.84 162 5833274 5.55 ug/L 98 17) Butachlor 26.66 160 1670748 5.51 ug/L 82 18) 4,4'-dde 2 7.29 246 1.570450 4.27 ug/L 100 22) Bis (2-Ethylhexyl) adipate 29.52 12 9 4148531 3.84 ug/L 99 23) Bis (2-Ethylhexyl) phthala 3 0.96 149 8215972 4.16 ug/L 99 24) Benzo (a) pyrene 34.17 252 6721555 5.25 ug/L 96
(#) = qualifier out of range (m) = manual integration 28318S.D 011402.M Tue Jan 15 14:13:33 2002 Page 1
NYC-WTC_000058051
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NYC-WTC_000058119
Reference standard analysis results for sample AD28048 showing pesticide compound responses on December 18, 2001.
1 shared topics · Same agency, volume and box · similarity 0.990
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000058069
Reference standard analysis results for sample AD28316 showing pesticide compound responses on January 17, 2002.
1 shared topics · Same agency, volume and box · similarity 0.989
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000058045
Reference standard analysis results for sample AD28319 showing pesticide compound responses on January 16, 2002.
1 shared topics · Same agency, volume and box · similarity 0.987
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000055831
Quality control report for reference standards (AD28322) verifying analytical precision on December 19, 2001.
1 shared topics · Same agency, volume and box · similarity 0.986
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000058053
Duplicate spike quality control analysis for EPA Method 525.2 pesticide screening on 1/16/2002, document image quality degraded.
1 shared topics · Same agency, volume and box · similarity 0.986
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000055814
Quality control report for reference standards (AD28847) verifying analytical precision on December 20, 2001.
1 shared topics · Same agency, volume and box · similarity 0.986
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000055111
Laboratory reference standard analysis for sample AD27547 showing measured values for pesticides and organic compounds.
1 shared topics · Same agency, volume and box · similarity 0.986
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000057734
Laboratory report listing analytical results for pesticides and organic compounds in recovery standard AD27547.
1 shared topics · Same agency, volume and box · similarity 0.986
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000055119
Laboratory analysis of spiked sample AD27547 showing recovery values for various pesticides and organic compounds.
1 shared topics · Same agency, volume and box · similarity 0.985
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000057742
Laboratory report listing analytical results for pesticides and organic compounds in spiked sample AD27547.
1 shared topics · Same agency, volume and box · similarity 0.984
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000055397
Quality control spiked sample results for Method 525.2 verifying recovery rates for target chemical compounds.
1 shared topics · Same agency, volume and box · similarity 0.984
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000057730
Laboratory report listing analytical results for pesticides and organic compounds in calibration standard AD27547.
1 shared topics · Same agency, volume and box · similarity 0.983
machine-extracted · confidence unavailable · Check page ↗No available related records indexed in this group.
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NYC-WTC_000057988
Laboratory report listing analytical results for pesticides and related compounds in sample AD26320 collected November 2001.
Filed in the same folder
NYC-WTC_000057989
Laboratory report listing analytical results for pesticides and related compounds in sample AD26320 collected November 2001.
Filed in the same folder
NYC-WTC_000057991
Data sheet recording water quality parameters including drip rate and pH for multiple sample IDs in December 2001.
Filed in the same folder
NYC-WTC_000057993
Instrument sequence log detailing the order of analysis for calibration standards and environmental samples in December 2001.
Filed in the same folder
NYC-WTC_000058015
Report verifying instrument calibration using standard compounds for Method 525.2 analysis in December 2001.
Filed in the same folder