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Document / 5 pages

Duplicate spike analysis, sample AD26534, Nov 2001

Machine-extracted title · confidence 90%

Laboratory report documenting results for a duplicate spiked sample of AD26534 to assess precision and reproducibility of the analytical method.

NYC-WTC_000057529–000057533

Folder label: “525 X 11/7/01 A 11/24/01

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2 2 K K O o 2o co _s

"0 1 o o o Integration Report Quanfile: 26434A Quan Entries: 17 C O o' o CM Comment: BOHLK; METHOD 525; INST 204; 11/24/01; SAMPLE 26434 "0 Sorted via: Entry Number 1 o CM — CD 0 D No Name of Compound R Time Scan# Mode Peak Area Pk Height o Q C 3 1 acenaphthene d-10(IS) 12:12 732 Auto 1,338,741 859,189 CD

2 phenanthrene d-10 CIS) 16:47 1007 Auto 1,932,677 694,895 3 chrysene d-12CIS) 22:35 1355 Auto 1,522,917 583,019 4 p-terphenyl d-14CIS) 20:46 1246 Auto 2,963,951 1,874,688 5 acenaphthene d-10CSURR 12:12 732 Auto 1,338,741 859,189 6 phenanthrene d-10CSURR 16:47 1007 Auto 1,932,677 694,895 7 chrysene d-12 CSURR) 22:35 1355 Auto 1,522,917 583,019 8 1,3-d imethy1-2-n itrobe 7:54 474 Auto 741,330 377,108 9 triphenyl phosphate CS 22:01 1321 Auto 939,924 456,093 10 perylene d-12 CSURR) 26:48 1608 Auto 864,932 169,860 11 hexachlorobenzene 15:12 912 Auto 5,801 2,243 12 b is C2-ethyIhexy1)ad ipa 22:01 1321 Auto 19,352 4,521 13 bis C2-ethyihexyl phtha 22:53 1373 Auto 600,063 201,726 14 2,6-d in itrotoluene 11:52 712 Auto 50,308 30,008 15 2,4-d in itrotoluene 13:00 780 Auto 4,385 1,920 16 butachlor 20:19 1219 Auto 1,395 1,395 17 4,4‘-dde 20:42 1242 Auto 3,949 3,099

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NYC-WTC_000057531Source: NYC Law Department, mirrored locally

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