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← Document results/DEP Box 30/508 X 11/15/01 A 12/12 - 12/13/01
Document / 7 pages

PCB calibration data, method 508, Nov-Dec 2001

Machine-extracted title · confidence 90%

Calibration data for PCB analysis using method 508, showing compound response factors.

NYC-WTC_000057187–000057193

Folder label: “508 X 11/15/01 A 12/12 - 12/13/01

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Scanned page image, NYC-WTC_000057188
OCR text

OCR status: ok · source: pdftotext

NYC 9/11 Public Portal Document Quantitation Report (QT Reviewed)

Signal 1 : C:\MSDCHEM\1\DATA\5O8\O11212B\CHLC2.D\ECD1A.CH Vial: 7 Signal 2 : C:\MSDCHEM\l\DATA\508\011212B\CHLC2.D\ECD2B.CH Acq On : 12 Dec 2001 4:56 pm Operator: Nefliu Sample : chi ic2 Inst : Instrume Mise : Multiplr: 1.00 IntFile Signal #1: • EVENTS.E IntFile Signal #2: events2.e Quant Time: Dec 26 14:44:32 2001 Quant Results File: 011212C.RES

Quant Method : C:\MSDCHEM\1\METHODS\011212C.M (Chemstation Integrator) Title : 508 Chlorinated Pesticides - Chlordane Last Update : Mon Dec 17 11:03:11 2001 Response via : Initial Calibration DataAcq Meth : MDL508.M

Volume Inj. Signal 1 Phase Signal 2 Phase: Signal 1 Info Signal 2 Info : Compound RT#1 RT#2 Resp#l Resp#2 ug/1 ug/1

System Monitoring Compounds 4) 3 2,4-DDD SURROGAT 14.34 14.98 688.8E6 489.4E6 0.200m 0.194m Spiked Amount 0.200 Recovery = 100.00% 97.00% Target Compounds 1) Chlordane Peak 1 10.80 10.88 359.2E6 260.4E6 1.610 1.612 2) Chlordane Peak 2 12.06 12.39 449.3E6 285.4E6 1.619 1.575 3) Chlordane Peak 3 13.42 13.76 1263.3E6 884.5E6 1.618m 1.638m

(f)=RT Delta > 1/2 Window (#)=Amounts differ by > 25% (m)=manual int. CHLC2.D 011212C.M Wed Dec 26 14:45:00 2001 Page 1

NYC-WTC_000057188

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NYC-WTC_000057188Source: NYC Law Department, mirrored locally

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