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Document / 7 pages

Pesticide control verification analysis, sample AD27546, Dec 2001

Machine-extracted title · confidence 95%

Lab quality control analysis verifying accuracy of pesticide detection methods for sample AD27546.

NYC-WTC_000057173–000057179

Folder label: “508 X 11/15/01 A 12/12 - 12/13/01

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Scanned page image, NYC-WTC_000057178
OCR text

OCR status: ok · source: pdftotext

NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed)

Signal 1 : C:\MSDCHEM\1\DATA\508\011212B\2TOXC2.D\ECD1A.CH Vial: 39 Signal 2 : C:\MSDCHEM\1\DATA\508\011212B\2TOXC2.D\ECD2B.CH Acq On : 13 Dec 2001 8:09 pm Operator: Nefliu Sample : tox ccv Inst : Instrume Mise : Multiplr: 1.00 IntFile Signal #1: EVENTS.E IntFile Signal #2: events2.e Quant Time: Dec 26 14:41:58 2001 Quant Results File: 011212T.RES

Quant Method : C:\MSDCHEM\1\METHODS\011212T.M (Chemstation Integrator) Title : 508 Chlorinated Pesticides - Toxaphene Last Update : Mon Dec 17 14:09:03 2001 Response via : Initial Calibration DataAcq Meth : MDL508.M

Volume Inj. Signal 1 Phase Signal 2 Phase: Signal 1 Info Signal 2 Info :

Compound RT#1 RT#2 Resp#l Resp#2 Conc#l Conc#2

System Monitoring Compounds 6) s 2,4-DDD SURROGAT 14.34 14.97 734.3E6 560.5E6 0.195m 0.214m / Spiked Amount 0.200 Recovery 97.50% 107.00% Target Compounds 1) Toxaphene Peak 1 14.75 15.70 186.4E6 76287605 3.399m 3.655m 2) Toxaphene Peak 2 15.12 16.12 244.6E6 403.OE6 3.392m 3.968m 3) Toxaphene Peak 3 15.52 16.28 130.7E6 129.2E6 3.264m 4.161m# 4) Toxaphene Peak 4 17.17 16.70 575.6E6 367.9E6 3.540m 3.914m 5) Toxaphene Peak 5 17.55 17.78 235.4E6 461.1E6 3.691m 4.246m .3< 1274)

(f)=RT Delta > 1/2 Window (#)=Amounts differ by > 25% (m)=manual int. 2TOXC2.D 011212T.M Wed Dec 26 14:43:01 2001 Page 1

NYC-WTC_000057178

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NYC-WTC_000057178Source: NYC Law Department, mirrored locally

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