Pesticide and contaminant analysis results, Nov-Dec 2001

NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed)

Data }le C:\MSDCHEM\l\DATA\120601\27274.D Vial: 39 Acq On 7 Dec 2001 9:49 pm Operator: McLean Sample 11/15 sample Inst : Instrumen Mise Multiplr: 1.00 MS Integation Params: BENZO. P Quant me: Dec 12 14:20:27 2001 Quant Results File: 120501.RES

Quant Mehod : C:\MSDCHEM\l\5973N\120501.M (RTE Integrator) Title : Quantitation For Method 525.2 Last ydate : Wed Dec 12 12:56:58 2001 Respose v^a : Initial Calibration Datanq Meth : 120501 Internal Standards R.T. Qlon Response Cone Units Dev(Min)

1) Acenaphthene-diO 18.32 164 6489059 5.00 ug/L 0.00 <) Phenanthrene D-10 22.65 188 10239422 5.00 ug/L 0.00 20) Chrysene D-12 30.43 240 6769488 5.00 ug/L 0.00

System Monitoring Compounds 2) 1,3-Dimethyl-2-nitrobenzen 13.23 134 1330626 3.86 ug/L 0.00 Spiked Amount 5.000 Recovery = 77.20% 19) Triphenyl Phosphate surr 29.70 326 2090042 5.89 ug/L 0.00 Spiked Amount 5.000 Recovery = 117.80% 21) Perylene D-12 surr 34.45 264 4355062 4.58 ug/L 0.00 Spiked Amount 5.000 Recovery = 91.60%

Target Compounds Qvalue 3) Hexachlorocyclopentadiene 0.00 237 0 N.D. 4) Hexachlorobenzene 21.52 284 21035 N.D. 5) EPTC 0.00 128 0 N.D. 6) 2,6-Dinitrotoluene 0.00 165 0 N.D. d 7) 2,4-Dinitotoluene 19.06 165 10719 0.32 ug/L # 21 8) Molinate 19.08 126 16396 N.D. 10) Simazine 0.00 201 0 N.D. 11) Atrazine 0.00 200 0 N.D. 12) Alachlor 0.00 160 0 N.D. 13) Terbacil 22.99 161 5310 N.D. 14) Acetochlor 0.00 146 0 N.D. 15) Metribuzin 0.00 198 0 N.D. 16) Metolachlor 0.00 162 0 N.D. 17) Butachlor 0.00 160 0 N.D. d 18) 4,4'-DDE 27.41 246 14629 N.D. 22) Bis (2-Ethylhexyl) adipate 29.62 129 81477 0.19 ug/L # 25 23) Bis (2-Ethylhexyl) phthala 31.07 149 605334 0.52 ug/L 99 24) Benzo (a) pyrene 0.00 252 0 N.D. d

(#) = qualifier out of range (m) = manual integration 27274.D 120501.M Wed Dec 12 14:21:09 2001 Page 1

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