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Pesticide analysis results below detection limits for sample AD28308

Machine-extracted title · confidence 100%

Laboratory report indicating pesticide concentrations were below method detection limits for sample AD28308 collected in late 2001.

NYC-WTC_000056866–000056874

Folder label: “508 X 11/26/01 A 12/21 - 12/22/01

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NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed)

Signal #1 : C:\MSDCHEM\1\DATA\508\011221B\28308.D\ECDlA.CH Vial: 43 Signal #2 : C:\MSDCHEM\1\DATA\508\011221B\28308.D\ECD2B.CH Acq On : 22 Dec 2001 8:27 am Operator: Nefliu Sample : sample Inst : Instrumen Mise : Multiplr: 1.00 IntFile Signal #1: EVENTS.E IntFile Signal #2: events2.e Quant Time: Jan 09 11:12:23 2002 Quant Results File: 011220P.RES

Quant Method : C:\MSDCHEM\1\METHODS\011220P.M (Chemstation Integrator) Title : 508 Chlorinated Pesticides Last Update : Fri Dec 21 08:18:43 2001 Response via : Initial Calibration DataAcq Meth : MDL508.M

Volume Inj. Signal #1 Phase Signal #2 Phase: Signal #1 Info Signal #2 Info :

Compound RT#1 RT#2 Resp#l Resp#2 ug/l ug/l

System Monitoring Compounds 10) S 2,4-DDD SURROGAT 14.35 14.98 603.0E6 452.8E6 0.163 0.162 Spiked Amount 0.200 Recovery = 81.50% 81.00%

Target Compounds 2) g-BHC 9.85 10.26 6421087 8990911 0.001 0.001 # 3) Heptachlor 11.00 11.25 3586922 4335000 0.000 0.001 # 4) Aldrin 11.69 0.00 5284411 0 0.001 N.D. d# 5) Heptachlor Epoxi 13.16 13.57 6341802 18138147 0.001 0.003 # 6) 4,4-DDE 13.96 14.17f 6008788 18308488 0.001 0.003 # 7) Dieldrin 14.54 0.00 4925253 0 0.001 N.D. d# 8) Endrin 0.00 15.81f 0 3404785 N.D. d 0.001 9) Methoxychlor 0.00 18.01 0 9915964 N.D. d 0.008

(f)=RT Delta > 1/2 Window (#)=Amounts differ by > 25% (m)=manual int. 28308.D 011220P.M Wed Jan 09 11:12:55 2002 Page 1

NYC-WTC_000056867

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NYC-WTC_000056867Source: NYC Law Department, mirrored locally

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