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← Document results/DEP Box 30/508 X 11/20/01 A 12/17/01 - 12/18/01
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Pesticide reference standard analysis, Sample AD27952, Nov-Dec 2001

Machine-extracted title · confidence 75%

Reference standard analysis ($RE508) for sample AD27952 showing most pesticides below detection limits except chlordane at 2.2 micrograms.

NYC-WTC_000056272–000056275

Folder label: “508 X 11/20/01 A 12/17/01 - 12/18/01

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Scanned page image, NYC-WTC_000056274
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NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed)

Signal #1 : C:\MSDCHEM\1\DATA\508\011217B\1120REFC.D\ECDlA.CH Vial: 16 Signal #2 : C:\MSDCHEM\1\DATA\508\011217B\1120REFC.D\ECD2B.CH Acq On : 17 Dec 2001 6:50 pm Operator: Nefliu Sample : 11/19 ref chi Inst : Instrumen Mise : Multiplr: 1.00 IntFile Signal #1: EVENTS.E IntFile Signal #2: events2.e Quant Time: Jan 04 13:52:19 2002 Quant Results File: 011214C.RES

Quant Method : C:\MSDCHEM\1\METHODS\011214C.M (Chemstation Integrator) Title : 508 Chlorinated Pesticides - Chlordane Last Update : Mon Dec 17 11:07:31 2001 Response via : Initial Calibration DataAcq Meth : MDL508.M

Volume Inj. Signal #1 Phase Signal #2 Phase: Signal #1 Info Signal #2 Info :

Compound RT#1 RT#2 Resp#l Resp#2 ug/1 ug/1

System Monitoring Compounds 4) s 2,4-DDD SURROGAT 14.34 14.97 603.9E6 507.3E6 0.173m 0.187 Spiked Amount 0.200 Recovery = 86.50% 93.50%

Target Compounds 1) Chlordane Peak 1 10.79 10.87 377.2E6 312.7E6 1.653m 1.690 2) Chlordane Peak 2 12.05 12.38 589.1E6 500.9E6 2.109m 2.499 3) Chlordane Peak 3 13.41 13.75 2143.8E6 1682.3E6 2.691m 2.794

19 X

(f)=RT Delta > 1/2 Window (#)=Amounts differ by > 25% (m)=manual int. 1120REFC.D 011214C.M Fri Jan 04 13:52:45 2002 Page 1

NYC-WTC_000056274

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NYC-WTC_000056274Source: NYC Law Department, mirrored locally

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