GC-MS analytical data and quality assurance results for polycyclic aromatic hydrocarbons and surrogate compounds with recovery analysis, Dec 18-19, 2001.
NYC-WTC_000055809–000055810Folder label: “525 X 11/27/01 A 12/17 - 12/18/01”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document Quantitation Report (QT Reviewed) A Data File : C:\MSDCHEM\1\DATA\121801\CCD.D Vial: 13 Acq On : 19 Dec 2001 4:54 am Operator: McLean Sample : 12.5 Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: BENZO.P Quant Time: Dec 19 05:31:05 2001 Quant Results File: 121401.RES
Quant Method : C:\MSDCHEM\l\5973N\121401.M (RTE Integrator) Title : Quantitation For Method 525.2 Last Update : Tue Dec 18 09:35:41 2001 Response via : Initial Calibration DataAcq Meth : 121401
Internal Standards R.T. Qlon Response Cone Units Dev(Min)
1) Acenaphthene-diO 18.21 164 8977024 5.00 ug/L 0.00 9) Phenanthrene D-10 22.53 188 12601938 5.00 ug/L 0.00 20) Chrysene D-12 30.31 240 9328772 5.00 ug/L 0.00
System Monitoring Compounds 2) 1,3-Dimethyl-2-nitrobenzen 13.13 134 2236768 4.87 ug/L 0.00 Spiked Amount 5.000 Recovery = 97.40% 19) Triphenyl Phosphate surr 29.58 326 2311835 6.03 ug/L 0.00 Spiked Amount 5.000 Recovery = 120.60% 21) Perylene D-12 surr 34.32 264 6419650 5.20 ug/L 0.00 Spiked Amount 5.000 Recovery = 104.00%
Target Compounds Qvalue 3) Hexachlorocyclopentadiene 15.71 237 3736879 14.70 ug/L 98 4) Hexachlorobenzene 21.41 284 6537105 11.01 ug/L 98 5) EPTC 16.18 128 10931328 12.79 ug/L 99 6) 2,6-Dinitrotoluene 17.78 165 5677404 12.75 ug/L 96 7) 2,4-Dinitotoluene 18.93 165 6788838 12.47 ug/L 98 8) Molinate 19.09 126 15633629 12.91 ug/L 99 10) Simazine 21.98 201 4808330 14.04 ug/L 98 11) Atrazine 22.08 200 6589133 14.72 ug/L 100 12) Alachlor 23.92 160 6067461 13.95 ug/L 93 13) Terbacil 22.94 161 8223960 15.58 ug/L 99 14) Acetochlor 23.71 146 4482108 14.16 ug/L 95 15) Metribuzin 23.76 198 7275440 11.91 ug/L 95 16) Metolachlor 24.84 162 20149351 14.37 ug/L 99 17) Butachlor 26.67 160 5850204 14.46 ug/L 83 18) 4,4'-DDE 27.30 246 5856724 11.93 ug/L 96 22) Bis (2-Ethylhexyl) adipate 29.52 129 18125235 10.91 ug/L 97 23) Bis (2-Ethylhexyl) phthala 30.95 149 22912362m <7.72 uq/L 24) Benzo (a) pyrene 34.17 252 24270307 13.21 ug/L 97
-16 2.19
(#) = qualifier out of range (m) = manual integration CCD.D 121401.M Thu Dec 20 09:32:18 2001 Page 1
NYC-WTC_000055809
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NYC-WTC_000055091
GC-MS analysis of polycyclic aromatic hydrocarbons and test compounds using EPA Method 525.2 with surrogate recoveries.
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Laboratory report for a lab blank sample AD27232 showing non-detect results for various pesticides.
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Calibration standard results for Method 525.2 listing concentrations and detection limits for target compounds.
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Data review document for a November 19 sample analyzed under Method 525 with recovery statistics.
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Quality control lab blank results for Method 525.2 showing detection limits for various pesticides and contaminants.
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Laboratory results for sample AD28044 analyzing pesticides and organic contaminants using Method 525.2.
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machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000055108
Calibration standard reference results for pesticide and organic compound analysis of sample AD27547, with measured values for 13 analytes including hexachlorobenzene (4.96 ug), si
1 shared topics · Same agency, volume and box · similarity 0.972
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000055828
Quality control report for calibration standards (AD28322) verifying instrument accuracy on December 19, 2001.
1 shared topics · Same agency, volume and box · similarity 0.972
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000058155
Instrument log showing retention times and recovery percentages for PAHs in a reference standard on January 28, 2002.
1 shared topics · Same agency, volume and box · similarity 0.971
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000030439
Analysis results for organic chemicals in sample AD27113 from site 525 collected between November and December 2001.
1 shared topics · similarity 0.975
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000012554
Laboratory report for sample AE11555 listing detection results for DDT and other pesticides in micrograms per unit.
1 shared topics · similarity 0.971
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