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Method 525 pesticide results, sample AD28323, Dec 2001

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Laboratory report listing pesticide and contaminant test results for sample AD28323 collected November 27, 2001.

NYC-WTC_000055800–000055803

Folder label: “525 X 11/27/01 A 12/17 - 12/18/01

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NYC 9/11 Public Portal Document Quantitation Report (QT Reviewed)

Data File : C:\MSDCHEM\1\DATA\121701\28323.D Vial: 29 Ac. J on : 17 Dec 2001 5:46 pm Operator: McLean . Sample : 112701 Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: BENZO.P Quant Time: Dec 17 18:23:31 2001 Quant Results File: 121401.RES

Quant Method : C:\MSDCHEM\l\5973N\121401.M (RTE Integrator) Title : Quantitation For Method 525.2 Last Update : Mon Dec 17 15:06:05 2001 Response via : Initial Calibration DataAcq Meth : 121401

Internal Standards R.T. Qlon Response Cone Units Dev(Min)

1) Acenaphthene-diO 18.20 164 5524108 5.00 ug/L 0.00 9) Phenanthrene D-10 22.53 188 8773844 5.00 ug/L 0.00 20) Chrysene D-12 30.30 240 6165390 5.00 ug/L 0.00

System Monitoring Compounds 2) 1,3-Dimethyl-2-nitrobenzen 13.13 134 1299797 4.60 ug/L 0.00 Spiked Amount 5.000 Recovery = 92.00% 19) Triphenyl Phosphate surr 29.58 326 1520475 5.69 ug/L 0.00 Spiked Amount 5.000 Recovery = 113.80% 21) Perylene D-12 surr 34.31 264 4345396 5.33 ug/L 0.00 Spiked Amount 5.000 Recovery = 106.60%

Target Compounds Qvalue 3) Hexachlorocyclopentadiene 0.00 237 0 N.D. 4) Hexachlorobenzene 0.00 284 0 N.D. d 5) EPTC 0.00 128 0 N.D. 6) 2,6-Dinitrotoluene 0.00 165 0 N.D. d 7) 2,4-Dinitotoluene 18.96 165 8898 0.33 ug/L # 21 8) Molinate 0.00 126 0 N.D. d 10) Simazine 0.00 201 0 N.D. 11) Atrazine 0.00 200 0 N.D. 12) Alachlor 0.00 160 0 N.D. 13) Terbacil 0.00 161 0 N.D. d 14) Acetochlor 0.00 146 0 N.D. 15) Metribuzin 0.00 198 0 N.D. 16) Metolachlor 0.00 162 0 N.D. 17) Butachlor 0.00 160 0 N.D. d 18) 4,4'-DDE 27.29 246 7699 0.02 ug/L 93 22) Bis (2-Ethylhexyl) adipate 29.52 129 15949 0.40 ug/L # 16 23) Bis (2-Ethylhexyl) phthala 30.95 149 193867 0.48 ug/L 95 24) Benzo (a) pyrene 0.00 252 0 N.D. d

(#) = qualifier out of range (m) = manual integration 28323.D 121401.M Wed Dec 19 15:50:50 2001 Page 1

NYC-WTC_000055801

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NYC-WTC_000055801Source: NYC Law Department, mirrored locally

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