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Spiked sample results, Method 525, Dec 2001

Machine-extracted title · confidence 90%

Spiked sample analysis for EPA Method 525.2 quality assurance showing measured recoveries for 20 compounds in sample AD27874.

NYC-WTC_000055264–000055268

Folder label: “525 X 11/20/01 A 12/6 - 12/7/01

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Scanned page image, NYC-WTC_000055267
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2 2 - - o o 2 CD — o “O I C o O o o Integration Report Quanfile: 27874MS Quan Entries: 28 o' o CH CH Comment: BOHLK; NETHOD 525; INST 204; 12/06/01; SANPLE 27874 MS "0 o N O. Sorted via: Entry Number t — 0 O No o Name of Compound R Time Scant Node Peak Area Pk Height Q C 3 CD 3 chrysene d-12(IS) 22:34 1354 Auto 3,543,117 1,808,359 4 p-terphenyl d-14(IS) 20:45 1245 Auto 7,240,159 3,892,505 5 acenaphthene d-10(SURR 12:11 731 Auto 3,259,247 2,114,506 6 phenanthrene d-10(SURR 16:46 1006 Auto 5,057,826 2,031,507 7 chrysene d-12 (SURE) 22:34 1354 Auto 3,543,117 1,808,359 8 1,3-d imethy1-2-n itrobe 7:53 473 Auto 1,697,382 865,576 9 triphenyl phosphate (S 22:00 1320 Auto 1,918,515 961,700 10 perylene d-12 (SURR) 26:45 1605 Auto 2,218,654 496,698 11 hexachlorocyclopentad i 10:02 602 Auto 593,941 355,434 12 hexachlorobenzene 15:11 911 Auto 1,533,187 683,914 13 simazine 15:58 958 Auto 822,408 226,542 14 atrazine 16:08 968 Auto 877,631 296,398 15 alachlor 18:17 1097 Auto 1,625,103 775,525 16 bis(2-ethyihexyl adipa 21:53 1313 Auto 2,287,158 1,348,550 17 b is(2-ethyIhexyl phtha 22:51 1371 Auto 4,436,646 2,217,487 18 benzo(a)pyrene 26:32 1592 Auto 2,905,208 645,000 19 eptc 18:28 628 Auto 6,292,101 3,037,385 P 20 2,6-d in itrotoluene 11:50 710 Auto 858,181 392,032 21 2,4-d in itrotoluene 12:49 769 Auto 881,476 420,574 22 molinate 12:56 776 Auto 2,434,763 1,213,169 23 terbac il 17:19 1039 Auto 1,816,819 494,089 24 acetochlor 18:06 1086 Auto 1,103,216 572,492 25 metribuzin 18:08 1088 Auto 1,248,225 663,000 26 metolachlor 19:03 1143 Auto 4,554,746 2,430,007 27 butachlor 20:18 1218 Auto 1,440,453 917,500 28 4,4‘dde 20:41 1241 Auto 1,753,235 1,359,426

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NYC-WTC_000055267Source: NYC Law Department, mirrored locally

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