NYC 9/11 Public Portal Document
> Data File : C:\HPCHEM\l\DATA\FEB1902\1335.D Vial: 9
Acq On : 19 Feb 2002 6:11 pm Operator: 209 GALOS
Sample : gc/ms scan 1/18 Inst : GC/MS 209
Mise : Multiplr: 1.00
MS Integration Params: GOOFY.P
Quant Time: Feb 21 14:36 2002 <Quant Results File: GCMS0208.RES
Quant Method : C:\HPCHEM\1\METHODS\GCMS0208.M (RTE Integrator)
Title : 209 625/TCLP calibration table
Last Update : Wed Feb 13 11:43:23 2002
Response via : Initial Calibration
DataAcq Meth : GCMS0208
Internal Standards R.T. Qlon Response Cone Units Dev(Min)
1) 1,4-Dichlorobenzene-d4 12.33 152 262836 20.00 ug/1 -0.02
10) Naphthalene-d8 15.97 136 1000075 20.00 ug/1 -0.03
17) Acenaphthene-dlO 21.29 164 515575 20.00 ug/1 -0.03
29) Phenanthrene-diO 25.74 188 715824 20.00 ug/1 -0.03
38) Chrysene-dl2 33.80 240 461884 20.00 ug/1 -0.05
44) Perylene-dl2 38.08 264 307499 20.00 ug/1 -0.05
System Monitoring Compounds
37) 2,4-DDD 30.81 235 35129 4.89 ug/mL 0.32
Spiked Amount 5.000 Recovery = 97.80%
Target Compounds Qvalue
2) N-nitroso-dimethyl amine 0.00 74 0 N.D.
3) bis(2-Chloroethyl)ether 0.00 93 0 . N.D.
4) 1,3-Dichlorobenzene 0.00 146 0 N.D.
5) 1,4-Dichlorobenzene 0.00 146 0 N.D.
6) 1,2-Dichlorobenzene 0.00 146 0 N.D.
7) 2,21 -oxybis(l-Chloropropan 0.00 45 0 N.D.
8) N-Nitroso-di-n-propylamine 0.00 70 0 N.D.
9) Hexachloroethane 0.00 117 0 N.D.
11) Nitrobenzene 0.00 77 0 N.D.
12) Isophorone 0.00 82 0 N.D.
13) bis(2-Chloroethoxy)methane 0.00 93 0 N.D.
14) 1,2,4-Trichlorobenzene 0.00 180 0 N.D.
15) Naphthalene 16.03 128 524 N.D.
16) Hexachlorobutadiene 0.00 225 0 N.D.
18) Hexachlorocyclopentadiene 0.00 237 0 N.D.
19) 2-Chloronaphthalene 0.00 162 0 N.D.
20) Dimethylphthalate 0.00 163 0 N.D.
21) 2,6-Dinitrotoluene 0.00 165 0 N.D.
22) Acenaphthylene 0.00 152 0 N.D.
23) Acenaphthene 0.00 153 0 N.D.
24) 2,4-Dinitrotoluene 0.00 165 0 N.D.
25) Diethylphthalate 22.75 149 351 N.D.
26) 4-Chlorophenyl-phenylether 0.00 204 0 N.D.
27) Fluorene 0.00 166 0 N.D.
28) Azobenzen/ 1,2-Diphenylhyd 0.00 77 0 N.D.
(#) = qualifier out of range (m) = manual integration
1335.D GCMS0208.M Thu Feb 21 14:37:27 2002 Page 1
NYC-WTC_000052946
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