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GCMS analysis results for sample AE01405, Feb 2002

Machine-extracted title · confidence 100%

Laboratory report documenting gas chromatography-mass spectrometry analysis of sample AE01405 conducted on February 27, 2002.

NYC-WTC_000052936–000052943

Folder label: “GCMS X 1/10/02 A 2/19/02

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NYC 9/11 Public Portal Document LSC Area Percent Report

. Data File : C:\HPCHEM\l\DATA\FEB1902\1405.D Vial: 14 Acq On : 19 Feb 2002 11:01 pm Operator: 209 GALOS Sample : gc/ms scan 1/18 Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\HPCHEM\1\METHODS\GCMS0208.M (RTE Integrator) Title : 209 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total

1 12.331 789 794 809 rVB 680912 1615708 71.18% 14.709% 2 15.976 1185 1191 1206 rBV 1028954 2133008 93.97% 19.419% 3 21.282 1763 1769 1784 rBV 1051706 2269768 100.00% 20.664% 4 25.734 2248 2254 2264 rBV2 1005656 2100440 92.54% 19.122% 5 30.811 2802 2807 2812 rBV 91430 175316 7.72% 1.596%

6 33.795 3126 3132 3146 rBV2 646459 1521962 67.05% 13.856% 7 38.082 3590 3599 3609 rBV2 389892 1168158 51.47% 10.635%

Sum of corrected areas: 10984360

1405.D GCMS0208 .M Thu Feb 21 15:30:30 2002

NYC-WTC_000052941

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NYC-WTC_000052941Source: NYC Law Department, mirrored locally

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