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GCMS analysis results for sample AE01333, Feb 2002

Machine-extracted title · confidence 100%

Laboratory report documenting gas chromatography-mass spectrometry analysis of sample AE01333 conducted on February 27, 2002.

NYC-WTC_000052892–000052900

Folder label: “GCMS X 1/10/02 A 2/19/02

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NYC 9/11 Public Portal Document

LSC Area Percent Report

Data File : C:\HPCHEM\l\DATA\FEB1902\1333.D Vial: 7 Acq On : 19 Feb 2002 4:15 pm Operator: 209 GALOS Sample : gc/ms scan 1/18 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\HPCHEM\1\METHODS\GCMS0208.M (RTE Integrator) Title : 209 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total

1 8.204 341 344 349 rBV2 10469 24920 1.32% 0.279% 2 12.335 788 794 804 rBV 540700 1344926 71.02% 15.039% 3 15.970 1184 1190 1205 rBV 854029 1771542 93.55% 19.809% 4 21.286 1763 1769 1777 rBV 956080 1893726 100.00% 21.175% 5 25.738 2248 2254 2264 rBV2 791132 1708402 90.21% 19.103%

6 30.815 2802 2807 2813 rVB 87824 174266 9.20% 1.949% 7 33.798 3126 3132 3142 rBV2 512762 1150894 60.77% 12.869% 8 38.076 3590 3598 3613 rBV2 287647 874363 46.17% 9.777%

Sum of corrected areas: 8943039

1333.D GCMS0208.M Thu Feb 21 15:26:25 2002

NYC-WTC_000052897

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NYC-WTC_000052897Source: NYC Law Department, mirrored locally

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