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GCMS calibration table for TCLP analysis, Feb 2002

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Technical document listing calibration standards and response factors for gas chromatography-mass spectrometry analysis of TCLP samples in February 2002.

NYC-WTC_000052884–000052891

Folder label: “GCMS X 1/10/02 A 2/19/02

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NYC 9/11 Public Portal Document

n Data File : C:\HPCHEM\1\DATA\FEB1902\1231.D Vial: 6 Acq On : 19 Feb 2002 3:17 pm Operator: 209 GALOS Sample : gc/ms scan 1/18 Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: Feb 21 14:23 2002 (Quant Results File: GCMS0208.RES

Quant Method : C:\HPCHEM\1\METHODS\GCMS0208.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Wed Feb 13 11:43:23 2002 Response via : Initial Calibration DataAcq Meth : GCMS0208

Compound R.T. Qlon Response Cone Unit Qvalue

30) N-Nitrosodiphenylamine 0.00 168 0 N.D. 31) 4-Bromophenyl-phenylether 0.00 248 0 N.D. 32) Hexachlorobenzene 0.00 284 0 N.D. 33) Phenanthrene 0.00 178 0 N.D. 34) Anthracene 0.00 178 0 N.D. 35) Di-n-butylphthalate 27.70 149 7435 N.D. 36) Fluoranthene 0.00 202 0 N.D. 39) Pyrene 0.00 202 0 N.D. 40) Butylbenzylphthalate 0.00 149 0 N.D. 41) Benzo(a)anthracene 33.79 228 944 N.D. 42) Bis(2-ethylhexyl)phthalate 34.00 149 926 N.D. 43) Chrysene 33.79 228 944 N.D. 45) Di-n-Octylphthalate 0.00 149 0 N.D. 46) Benzo(b)fluoranthene 0.00 252 0 N.D. 47) Benzo(k)fluoranthene 0.00 252 0 N.D. 48) Benzo(a)pyrene 38.09 252 1163 N.D. 49) Indeno(1,2,3-cd)pyrene 0.00 276 0 N.D. 50) Dibenz(a,h)anthracene 0.00 278 0 N.D. 51) Benzo(g,h,i)perylene 0.00 276 0 N.D.

(#) = qualifier out of range (m) = manual integration 1231.D GCMS0208.M Thu Feb 21 14:30:29 2002 Page 2

NYC-WTC_000052885

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NYC-WTC_000052885Source: NYC Law Department, mirrored locally

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