GCMS analysis report for sample AE01226, Feb 2002

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GC/MS analysis report for sample AE01226 showing surrogate recovery data generated on February 25, 2002.

NYC-WTC_000052805–000052814

Folder label: “GCMS X 1/17/02 A 2/16/02”

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Data File : C:\HPCHEM\l\DATA\FEB1502\1226.D Vial: 26 Acq On : 16 Feb 2002 5:38 pm Operator: 209 GALOS Sample : gc/ms scan 1/17 Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: Feb 20 14:03 2002 <Quant Results File: GCMS0208.RES

Quant Method : C:\HPCHEM\1\METHODS\GCMS0208.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Wed Feb 13 11:43:23 2002 Response via : Initial Calibration DataAcq Meth : GCMS0208

Internal Standards R.T. Qlon Response Cone Units Dev(Min)

1) 1,4-Dichlorobenzene-d4 12.33 152 280458 20.00 ug/1 -0.02 10) Naphthalene-d8 15.97 136 1046318 20.00 ug/1 -0.02 17) Acenaphthene-dlO 21.29 164 565470 20.00 ug/1 -0.02 29) Phenanthrene-dlO 25.73 188 817180 20.00 ug/1 -0.03 38) Chrysene-dl2 33.80 240 543083 20.00 ug/1 -0.04 44) Perylene-dl2 38.08 264 354389 20.00 ug/1 -0.04

System Monitoring Compounds 37) 2,4-DDD 30.81 235 43656 5.32 ug/mL 0.31 Spiked Amount 5.000 Recovery = 106.40%

Target Compounds 2) N-nitroso-dimethyl amine 3) bis(2-Chloroethyl)ether 4) 1,3-Dichlorobenzene 5) 1,4-Dichlorobenzene 6) 1,2-Dichlorobenzene 7) 2,2‘-oxybis(1-Chloropropan 8) N-Nitroso-di-n-propylamine 9) Hexachloroethane 11) Nitrobenzene 12) Isophorone 13) bis(2-Chloroethoxy)methane 14) 1,2,4-Trichlorobenzene 15) Naphthalene 16) Hexachlorobutadiene 18) Hexachlorocyclopentadiene 19) 2-Chloronaphthalene 20) Dimethylphthalate 21) 2,6-Dinitrotoluene 22) Acenaphthylene 23) Acenaphthene 24) 2,4-Dinitrotoluene 25) Diethylphthalate 26) 4-Chlorophenyl-phenylether 27) Fluorene 28) Azobenzen/ 1,2-Diphenylhyd Qvalue 0.00 74 0 N.D. 0.00 93 0 N.D. 0.00 146 0 N.D. 0.00 146 0 N.D. 0.00 146 0 N.D. 0.00 45 0 N.D. 0.00 70 0 N.D. 0.00 117 0 N.D. 13.53 77 542 N.D. 0.00 82 0 N.D. 0.00 93 0 N.D. 0.00 180 0 N.D. 16.03 128 630 N.D. 0.00 225 0 N.D. 0.00 237 0 N.D. 0.00 162 0 N.D. 0.00 163 0 N.D. 0.00 165 0 N.D. 0.00 152 0 N.D. 0.00 153 0 N.D. 0.00 165 0 N.D. 22.76 149 606 N.D. 0.00 204 0 N.D. 0.00 166 0 N.D. 0.00 77 0 N.D.

(#) = qualifier out of range (m) = manual integration 1226.D GCMS0208.M Wed Feb 20 14:04:48 2002 Page 1

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