GCMS analysis report for sample AE01038, Feb 2002

NYC 9/11 Public Portal Document

yuancitation Report (QT Reviewed)

Data File : C:\HPCHEM\1\DATA\FEB1102\1038.D Vial: 26 Acq On : 12 Feb 2002 10:30 am Operator: 209 GALOS Sample : GC/MS SCAN 1/15 Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: Feb 19 10:15 2002 (Quant Results File: GCMS0208.RES

Quant Method : C:\HPCHEM\1\METHODS\GCMS0208.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Wed Feb 13 11:43:23 2002 Response via : Initial Calibration DataAcq Meth : GCMS0208

Internal Standards R.T. Qlon Response Cone Units Dev(Min)

1) 1,4-Dichlorobenzene-d4 12.34 152 261086 20.00 ug/1 -0.01 10) Naphthalene-d8 15.99 136 994726 20.00 ug/1 -0.01 17) Acenaphthene-diO 21.30 164 539758 20.00 ug/1 -0.01 29) Phenanthrene-dlO 25.76 188 789403 20.00 ug/1 -0.01 38) Chrysene-dl2 33.83 240 554159 20.00 ug/1 -0.02 44) Perylene-dl2 38.11 264 342853 20.00 ug/1 -0.01

System Monitoring Compounds 37) 2,4-DDD 30.83 235 49697 6.27 ug/mL 0.33 Spiked Amount 5.000 Recovery = 125.40%

Target Compounds Qvalue 2) N-nitroso-dimethyl amine 0.00 74 0 N.D. 3) bis(2-Chloroethyl)ether 0.00 93 0 N.D. 4) 1,3-Dichlorobenzene 0.00 146 0 N.D. 5) 1,4-Dichlorobenzene 0.00 146 0 N.D. 6) 1,2-Dichlorobenzene 0.00 146 0 N.D. 7) 2,21-oxybis(1-Chloropropan 0.00 45 0 N.D. 8) N-Nitroso-di-n-propylamine 0.00 70 0 N.D. 9) Hexachloroethane 0.00 117 0 N.D. 11) Nitrobenzene 0.00 77 0 N.D. 12) Isophorone 0.00 82 0 N.D. 13) bis(2-Chloroethoxy)methane 0.00 93 0 N.D. 14) 1,2,4-Trichlorobenzene 0.00 180 0 N.D. 15) Naphthalene 16.05 128 603 N.D. 16) Hexachlorobutadiene 0.00 225 0 N.D. 18) Hexachlorocyclopentadiene 0.00 237 0 N.D. 19) 2-Chloronaphthalene 0.00 162 0 N.D. 20) Dimethylphthalate 0.00 163 0 N.D. 21) 2,6-Dinitrotoluene 0.00 165 0 N.D. 22) Acenaphthylene 0.00 152 0 N.D. 23) Acenaphthene 0.00 153 0 N.D. 24) 2,4-Dinitrotoluene 0.00 165 0 N.D. 25) Diethylphthalate 22.78 149 245 N.D. 26) 4-Chlorophenyl-phenylether 0.00 204 0 N.D. 17) Fluorene 0.00 166 0 N.D. :8) Azobenzen/ 1,2-Diphenylhyd 0.00 77 0 N.D.

) = qualifier out of range (m) = manual integration 38 .D GCMS0208.M Tue Feb 19 10:16:37 2002 Page 1

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