GC/MS procedural blank analysis results showing non-detectable levels of target organic compounds, confirming clean analytical conditions.
NYC-WTC_000052685–000052692Folder label: “GCMS X 1/15/02 A 2/11/02”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document
Quantitation Report (QT Reviewed)
Data File : C:\HPCHEM\l\DATA\FEB1102\LBA.D Vial: 16 Acq On : 12 Feb 2002 12:49 am Operator: 209 GALOS Sample : GC/MS SCAN 1/15 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: Feb 19 9:43 2002 Quant Results File: GCMS0208.RES
Quant Method : C:\HPCHEM\1\METHODS\GCMS0208.M (RTE Integrator) Title :.209 625/TCLP calibration table Last Update : Wed Feb 13 11:43:23 2002 Response via : Initial Calibration DataAcq Meth : GCMS0208
Internal Standards R.T. Qlon Response Cone Units Dev(Min)
1) l,4-Dichlorobenzene-d4 12.34 152 278656 20.00 ug/1 0.00 10) Naphthalene-d8 15.99 136 1064021 20.00 ug/1 0.00 17) Acenaphthene-diO 21.30 164 571658 20.00 ug/1 0.00 29) Phenanthrene-diO 25.76 188 824627 20.00 ug/1 0.00 38) Chrysene-dl2 33.83 240 551606 20.00 ug/1 -0.02 44) Perylene-d12 38.11 264 341002 20.00 ug/1 0.00
System Monitoring Compounds 37) 2,4-DDD 30.83 235 43310 5.23 ug/mL 0.34 Spiked Amount 5.000 Recovery = 104.60%
Target Compounds Qvalue 2) N-nitroso-dimethyl amine 0.00 74 0 N.D. 3) bis(2-Chloroethyl)ether 0.00 93 0 N.D. 4) 1,3-Dichlorobenzene 0.00 146 0 N.D. 5) 1,4-Dichlorobenzene 0.00 146 0 N.D. 6) 1,2-Dichlorobenzene 0.00 146 0 N.D. 7) 2,2'-oxybis(1-Chloropropan 0.00 45 0 N.D. 8) N-Nitroso-di-n-propylamine 0.00 70 0 N.D. 9) Hexachloroethane 0.00 117 0 N.D. 11) Nitrobenzene 0.00 77 0 N.D. 12) 1sophorone 0.00 82 0 N.D. 13) bis(2-Chloroethoxy)methane 0.00 93 0 N.D. 14) 1,2,4-Trichlorobenzene 0.00 180 0 N.D. 15) Naphthalene 16.04 128 715 N.D. 16) Hexachlorobutadiene 0.00 225 0 N.D. 18) Hexachlorocyclopentadiene 0.00 237 0 N.D. 19) 2-Chloronaphthalene 0.00 162 0 N.D. 20) Dimethylphthalate 0.00 163 0 N.D. 21) 2,6-Dinitrotoluene 0.00 165 0 N.D. 22) Ac enapht hylene 0.00 152 0 N.D. 2 3) Acenaphthene 0.00 153 0 N.D. 24) 2,4-Dinitrotoluene 0.00 165 0 N.D. 25) Diethylphthalate 22.79 149 314 N.D. 26) 4-Chlorophenyl-phenylether 0.00 204 0 N.D. 27) Fluorene 0.00 166 0 N.D. 28) Azobenzen/ 1,2-Diphenylhyd 0.00 77 0 N.D.
) = qualifier out of range (m) = manual integration A.D GCMS0208.M Tue Feb 19 09:44:13 2002 Page 1
NYC-WTC_000052686
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NYC-WTC_000052600
Calibration record for GC/MS instrument 209 used in TCLP testing, listing standard compounds and response factors from February 14, 2002.
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GC/MS blank analysis report for sample AE01041 showing volatile organic compound results generated on February 20, 2002.
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Gas chromatography-mass spectrometry blank control analysis showing all organic contaminants below method detection limits for quality assurance.
1 shared topics · similarity 0.992
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000003705
Blank sample results showing non-detect levels for volatile organic compounds during GCMS testing on February 28, 2002.
1 shared topics · similarity 0.991
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000003832
Gas chromatography-mass spectrometry blank control results for sample AE01937, confirming all tested organic compounds are below minimum detection limits.
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Laboratory report of a GCMS blank run for sample AD31347 performed on February 5, 2002.
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Blank analysis report for DEP sample AE02966 showing all target compounds below minimum detection limits.
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Laboratory data table recording drip rates and volumes for GCMS Method 508 analysis.
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machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000005756
Blank analysis report showing non-detectable levels of volatile organic compounds in laboratory reagents on February 15, 2002.
1 shared topics · similarity 0.989
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000016799
GCMS blank analysis results for sample AD30009 dated January 7, 2002, showing detection limits for various compounds.
1 shared topics · similarity 0.988
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000016506
Blank analysis report for DEP sample AD31363 showing non-detect levels for volatile organic compounds from February 7, 2002.
1 shared topics · similarity 0.987
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000016285
Laboratory report of a GCMS blank run performed on February 7, 2002, to verify absence of contamination.
1 shared topics · similarity 0.987
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NYC-WTC_000052672
Document header or index page from the GCMS X series folder covering samples analyzed between January and February 2002.
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NYC-WTC_000052673
Document header or index page from the GCMS X series folder covering samples analyzed between January and February 2002.
Filed in the same folder
NYC-WTC_000052676
Calibration report for GCMS analysis of volatile organic compounds including nitrosamines and chlorinated solvents from February 2002.
Filed in the same folder
NYC-WTC_000052680
Calibration report for GCMS analysis of volatile organic compounds including nitrosamines and chlorinated solvents from February 2002.
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NYC-WTC_000052693
Laboratory report documenting GCMS analysis of sample AE00945 conducted on February 26, 2002.
Filed in the same folder