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GCMS analysis results for sample AE01047, March 2002

Machine-extracted title · confidence 100%

Laboratory report documenting GCMS analysis of sample AE01047 conducted on March 14, 2002.

NYC-WTC_000052653–000052665

Folder label: “GCMS X 1/15/02 A 2/28/02

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Scanned page image, NYC-WTC_000052658
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NYC 9/11 Public Portal Document

Data File : C:\MSDCHEM\l\DATA\022802\01047FB.D Vial: 16 Acq On : 28 Feb 2002 11:15 pm Operator: McLean Sample : GC MS SCAN 2/27 Inst Instrumen Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\MSDCHEM\l\5973N\5080202.M (RTE Integrator) Title : Quantitation For Method 508gcscan Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak corr. corr. % of # min scan scan scan TY height area % max. total

1 9.570 711 716 741 rBV 1638017 4302381 67.10% 11.785% 2 12.083 988 993 999 rVB 226890 377849 5.89% 1.035% 3 13.053 1095 1100 1115 rBV 3074611 5876925 91.66% 16.098% 4 18.160 1657 1663 1673 rBV 3293013 6271214 97.81% 17.178% 5 22.523 2138 2144 2158 rBV2 3086440 6411891 100.00% 17.564%

6 27.457 2684 2688 2698 rBV 549820 1006414 15.70% 2.757% 7 30.332 2998 3005 3019 rBV2 2840923 6324870 98.64% 17.325% 8 34.205 3425 3432 3441 rBV2 1919868 4880156 76.11% 13.368% 9 35.683 3591 3595 3604 rVB2 101482 298183 4.65% 0.817% 10 36.427 3672 3677 3686 rVB2 170820 471699 7.36% 1.292%

11 37.416 3782 3786 3795 rW6 45846 111974 1.75% 0.307% 12 37.543 3797 3800 3809 rVB9 31013 106344 1.66% 0.291% 13 38.314 3880 3885 3895 rVBlO 19676 66481 1.04% 0.182%

Sum of corrected areas: 36506381

047FB.D 5080202.M Wed Mar 13 11:03:28 2002 Page 1

NYC-WTC_000052658

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NYC-WTC_000052658Source: NYC Law Department, mirrored locally

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