GCMS analysis results for sample AE01004, March 2002

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Laboratory report documenting GCMS analysis of sample AE01004 conducted on March 14, 2002.

NYC-WTC_000052592–000052599

Folder label: “GCMS X 1/15/02 A 2/28/02”

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NYC 9/11 Public Portal Document yuautitatlon Report (QT Reviewed) Dat File : c:\MSDCHEM\I\DATA\022802\01004. Vial: 9 Acq On : 28 Feb 2002 5:32 pm Operator: McLean J Sample : GC MS SCAN 2/27 Inst : Instrumen Mise : Multiplr: 1.00 MS Integration Params: BENZO.P Quant Time: Mar 13 10:57:37 2002 Quant Results File: 5080202.RES

Quant Method : C:\MSDCHEM\l\5973N\5080202.M (RTE Integrator) Title : Quantitation For Method 508gcscan Last Update : Mon Feb 25 19:17:14 2002 Response via : Initial Calibration DataAcq Meth : 508SCAN

Internal Standards R.T. Qlon Response Cone Units Dev(Min)

1) 1,4-Dichlorobenzene-d4 9.58 150 1340111 20.00 ug/L 0.00 10) Naphthalene-d8 13.05 136 3548191 20.00 ug/L 0.00 17) Acenaphthene-dlO 18.17 164 1975323 20.00 ug/L 0.00 29) Phenanthrene-dlO 22.52 188 3065486 20.00 ug/L 0.00 38) Chrysene-dl2 30.34 240 2794278 20.00 ug/L -0.02 44) Perylene-dl2 34.21 264 1833874 20.00 ug/L 0.00

System Monitoring Compounds 37) 2,4-ddd surr 27.46 235 277906 5.71 ug/L 0.00 Spiked Amount 5.000 Recovery = 114.20%

Target Compounds Qvalue 2) N-nitroso-dimethyl amine 0.00 74 0 N.D. d 3) bis(2-chloroethyl) ether 0.00 93 0 N.D. 4) 1,3 - Dichlorobenze 0.00 146 0 N.D. 5) 1,4 - Dichlorobenzene 0.00 146 0 N.D. 6) 1,2 - Dichlorobenzene 0.00 146 0 N.D. 7) 2,2 ' - oxybis (l-Chloropr 0.00 45 0 N.D. 8) N-Nitroso-di-n-propylamine 0.00 70 0 N.D. 9) Hexachloroethane 0.00 117 0 N.D. 11) Nitrobenzene 0.00 77 0 N.D. 12) Isophorone 0.00 82 0 N.D. 13) bis (2-hloroethoxy) methan 0.00 93 0 N.D. 14) 1,2,4-trichlorobenzene 0.00 180 0 N.D. 15) Naphthlene 0.00 128 0 N.D. 16) HexacHorobutadiene 0.00 225 0 N.D. 18) Hexacltorocyclopentadiene 0.00 237 0 N.D. 19) 2-chlconaphthalene 0.00 162 0 N.D. 20) Dimetllphthalate 0.00 163 0 N.D. 21) 2,6-Diitrotoluene 0.00 165 0 N.D. d 22) Acenajthylene 0.00 152 0 N.D. 23) Acenajthene 0.00 153 0 N.D. 24) 2,4-Ditrotoluene 0.00 165 0 N.D. 25) Diethyhthalate 0.00 149 0 N.D. 26) 4-Chlophenyl-phenyl ethe 0.00 204 0 N.D. 27) Fluore 0.00 166 0 N.D. 28) Azobenn/ 1,2-Diphenylhyd 0.00 77 0 N.D. 30) N-Nitrodiphenylamine 0.00 169 0 N.D. 31) 4-Bronhenyl-phenyl ether 0.00 248 0 N.D. 32) Hexackrobenzene 0.00 284 0 N.D. 33) Phenamrene 0.00 178 0 N.D. 34) Anthrae 0.00 178 0 N.D. 35) Di-n-blphthalate 24.67 149 2812 0.01 ug/L 79 36) Fluoraene 0.00 202 0 N.D. 39) Pyrene 0.00 202 0 N.D. 40) Butylbylphthalate 0.00 149 0 N.D. 41) Benzo antracene 0.00 228 0 N.D. d 42) Bis (2iylhexyl) phthala 30.94 149 4934 0.04 ug/L 85 43) Chrysei 0.00 228 0 N.D. d 45) Di-n-Ophthalate 0.00 149 0 e 2 N.D. 46) Benzo fluoranthene 0.00 252 0 N.D. #) = qualii out of range (m) = manual integration 1004.D 50%.M Wed Mar 13 10:58:43 2002 Page 1

NYC-WTC_000052594

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NYC-WTC_000052594Source: NYC Law Department, mirrored locally

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