GCMS analysis report for sample AE01002, Mar 2002

z Z K K o 3 o o CD — I "0 o C o O o o o' CH VUciit X tat.Oli RCpOL UL RvLwSw/ N "0 CH o N — Data File : C:\MSDCHEM\l\DATA\022802\0226REFA.D Vial: 3 0 Acq On : 28 Feb 2002 12:38 pm Operator: McLean O Sample : GC MS SCAN 2/27 Inst : Instrumen o Q C Mise : Multiplr: 1.00 3 MS Integration Params: BENZO.P CD Quant Time: Mar 13 6:41 2002 Quant Results File: 5080202.RES

Method : C:\MSDCHEM\l\5973N\5080202.M (RTE Integrator) Title : Quantitation For Method 508gcscan Last Update : Mon Feb 25 19:17:14 2002 Response via : Initial Calibration Abundance TIC: 0226REFA.D

4000000 o CM $O y4) o £ 6 80 86 V 8 2 3500000 8 6 " 1 i £ .

3000000 I I

I 8N [ 5O 8 8 2500000 8 o CI s Q.

9 ! 5 D 5 9 8 (o IB 2000000 £ 88 d 8 o 5 0) 86 g l O 8 (Q 8 E ra £ B s tg 11 2 d S J 2 £ s8 22 1 2 s *5% E 5 a 6 8 5 5 5 5 £ & ■ co 5. E Q 2 P 1500000 o 8 « s 15 8& N o F w t 8 8 81 £ 5 0 £ 7 6 2 O

a &2 | s.! 8 88 a £ 9 8 0E $ o 88 581 8 £ 8 55, 155 8 S } 8 v 53 « ® s.

1000000 a 685 Ijpfl O v 6 N I§ 2 0 9 5 a C & $ 2 c® o e e os.F8 “=2 £8 8 18 CO i s. -1 5-1 4 8 § 8 V 88 — 8 8 cm" c co

500000 § .8 3 58$ CM 5 ’ I 8 3 8 ef

I 8 8 6 6 s 8 z 5 2 4 2

Time--> 0--mm-PI 4.00 6.00 8.00 10.00 —L 12.00 rp 14.00 — —16.001UK 18.00 20.00 22.00 24.00 26.00 28.00 TL 30.00 32.00 I 34.00 36.00 38.00

0226REFA.D 5080202.M Wed Mar 13 06:42:10 2002 Page 3