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GCMS analysis results for sample AE00949, Feb 27 2002

Machine-extracted title · confidence 95%

Laboratory report detailing GCMS scan results for sample AE00949, including detection of unknown compounds and surrogate recovery data.

NYC-WTC_000052388–000052395

Folder label: “GCMS X 1/14/02 A 2/22 - 2/23/02

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Scanned page image, NYC-WTC_000052393
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NYC 9/11 Public Portal Document LSC Area Percent Report

Data File : C:\MSDCHEM\l\DATA\022202\0949.D Vial: 16 . Acq On : 23 Feb 2002 1:17 am Operator: McLean Sample : 1/14/02 Inst Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\MSDCHEM\l\5973N\5080202.M (RTE Integrator) Title : Quantitation For Method 508gcscan Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak corr. corr. % of # min scan scan scan TY height area % max. total

1 9.579 712 717 732 rBV 1552821 3913470 68.80% 12.534% 2 13.053 1095 1100 1116 rBV 2912993 5414527 95.19% 17.341% 3 18.160 1658 1663 1674 rBV 2913567 5656540 99.45% 18.116% 4 22.523 2138 2144 2154 rBV2 2808873 5687888 100.00% 18.217% 5 27.457 2684 2688 2695 rBV 330842 599170 10.53% 1.919%

6 30.332 2999 3005 3019 rBV2 2513857 5629370 98.97% 18.029% 7 34.214 3426 3433 3451 rBV 1878896 4322231 75.99% 13.843%

Sum of corrected areas: 31223196

1949.D 5080202.M Wed Feb 27 08:32:49 2002 Page 1

NYC-WTC_000052393

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NYC-WTC_000052393Source: NYC Law Department, mirrored locally

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