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GCMS analysis results for sample AE00832, Feb 4 2002

Machine-extracted title · confidence 90%

Laboratory report showing GCMS analysis of sample AE00832 including surrogate recovery and unknown compounds.

NYC-WTC_000052147–000052166

Folder label: “GCMS X 1/11/02 A 1/31/02

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Scanned page image, NYC-WTC_000052149
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NYC 9/11 Public Portal Document

Quantitation Report (Not Reviewed) Data' File : C:\MSDCHEM\1\5973N\02JAN31\00832.D Vial: 5 Acq On : 31 Jan 2002 1:52 pm Operator: Sample : 508 scan Inst : Instrumen Mise : January 31, 2002 Multiplr: 1.00 MS Integration Params: SPLIT.P Quant Time: Feb 01 08:46:03 2002 Quant Results File: SCAN508.RES Quant Method : C:\MSDCHEM\l..-\SCAN508.M (RTE Integrator) Title : 508 scan method Last Update : Fri Jan 11 13:20:07 2002 Response via : Initial Calibration DataAcq Meth : SCAN508

Internal Standards R.T. Qlon Response Cone Units Dev(Min) 1) 1,4-Dichlorobenzene-d4 9.71 152 1903553 20.00 ug/L 0.00 10) Naphthalene-d8 13.19 136 8111995 20.00 ug/L -0.02 17) Acenaphthene-diO 18.34 164 4233932 20.00 ug/L -0.01 29) Phenanthrene-diO 22.65 188 6685511 20.00 ug/L -0.02 38) Chrysene-dl2 30.50 240 5613880 20.00 ug/L -0.01 44) Perylene-dl2 34.42 264 4082181 20.00 ug/L 0.00 System Monitoring Compounds 37) 2,4-DDD 27.73 235 459141 4.34 ug/L 0.00 Spiked Amount 5.000 Recovery = 86.80% Target Compounds Qvalue 21) 2,6-Dinitrotoluene 18.34 165 532807 9.77 ug/L # 17 42) Bis(2-ethylhexyl)phthalate 31.11 149 22272 0.63 ug/L 92

(#) = qualifier out of range (m) = manual integration 00832.D SCAN508.M Fri Feb 01 08:46:04 2002 Page 1

NYC-WTC_000052149

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NYC-WTC_000052149Source: NYC Law Department, mirrored locally

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