DEP sample preparation log fragment, Jan-Feb 2002

NYC 9/11 Public Portal Document

DFTPP 7 Data File : C:\MSDCHEM\1\5973N\02JAN31\0131DF.D Vial: 1 Acq On : 31 Jan 2002 8:43 am Operator: Sample : dftpp Inst : Instrume Mise : January 31, 2002 Multiplr: 1.00 MS Integration Params: SPLIT.P Method : C:\MSDCHEM\1\METHODS\METHODS\SC7XN508.M (RTE Integrator) Title : 508 scan method

Abundance TIC: 0131 DF.D

6000000

5000000

4000000

3000000

2000000

1000000

0 i IT—mu | < > | | r i > | t IMI-T i > i i p i i i p i i l p ■ ■ i p ■ ■ i । ■ i । > f > l p 111111 1141*******’***—* Time-> 4.00 6.00 8.00 10.00 12.00 14.00 16.00 18.00 20.00 22.00 24 00 26.00 28.00 30.00 32.00 34.00 36.00 38.00 Abundance Average of 24.118 to 24.141 min.: 0131 DF.D 198 500000 442

400000

300000 127 255 77 51 200000 110 275 100000 224 296 A— 323 346 365 383 403 423 93 [ 148 167, /z-> o 37+4 4 rr' ■111 ■ 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 380 400 420 440 f ' ' FTi < » । । | i > i • | i k i । | ' । . r | • i

Spectrum Information: Average of 24.118 to 24.141 min.

Target Rei. to Lower Upper Rei. Raw Result Mass Mass Limit% Limit% Abn% Abn Pass/Fail

51 198 30 60 43.0 232874 PASS 68 69 0.00 2 0.5 1134 PASS 69 198 0.00 100 38.9 210858 PASS 70 69 0.00 2 0.5 1132 PASS 127 198 40 60 52.6 285184 PASS 197 198 0.00 1 0.0 0 PASS 198 198 100 100 100.0 541824 PASS 199 198 5 9 6.5 35112 PASS 275 198 10 30 22.1 119605 PASS 365 198 1 99 2.6 14278 PASS 441 443 1 99 75.7 73469 PASS 442 198 40 110 90.6 490858 PASS 443 442 17 23 19.8 97093 PASS

0131DF.D SCAN508.M Thu Jan 31 10:19:40 2002

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