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GCMS results for sample AE00700, Feb 13 2002

Machine-extracted title · confidence 100%

GCMS analysis log for sample AE00700 showing surrogate recovery and unknown compounds detected on February 13, 2002.

NYC-WTC_000051806–000051824

Folder label: “GCMS X 1/10/02 A 1/16/02

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Scanned page image, NYC-WTC_000051808
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NYC 9/11 Public Portal Document Quantitation Report (QT Reviewed) 15973020100700. Vial: 7 Dat - Feb 2002 7:42 pm Operator: Aco Fil 8 scan Inst : Instrumen San, debruary 1, 2002 Multiplr: 1.00 Mis. ion Params: SPLIT.P Ms e: Feb 04 09:24:38 2002 Quant Results File: SCAN508.RES ” : C:\MSDCHEM\1...\SCANS0B.M (RTE Integrator) Qua,Method Que 3t Update : : 508 scan method Fri Jan 11 13:20:07 2002 /-@xk esponse via : Initial Calibration DataAcq Meth : SCAN508 Internal Standards R.T. Qlon Response Cone Units Dev(Min) 1) 1,4-Dichlorobenzene-d4 9.71 152 1359667 20.00 ug/L 0.00 10) Naphthalene-d8 13.19 136 5816571 20.00 ug/L -0.02 17) Acenaphthene-diO 18.34 164 3083377 20.00 ug/L -0.01 29) Phenanthrene-dlO 22.63 188 5179354 20.00 ug/L -0.03 38) Chrysene-dl2 30.49 240 4326426 20.00 ug/L -0.02 44) Perylene-dl2 34.42 264 2941371 20.00 ug/L 0.00 System Monitoring Compounds 37) 2,4-DDD 27.73 235 313530 3.83 ug/L 0.00 Spiked Amount 5.000 Recovery = 76.60% Target Compounds Qvalue 42) Bis(2-ethylhexyl)phthalate 31.11 149 15984 0.62 ug/L 98

+) = qualifier out of range (m) = manual integration >700.D SCAN508.M Mon Feb 04 0 9 : 25 : 2 3 2 0 0 2 Page 1

NYC-WTC_000051808

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NYC-WTC_000051808Source: NYC Law Department, mirrored locally

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