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GCMS surrogate recovery results for sample AE00316, Jan 2002

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Laboratory record documenting GCMS surrogate recovery data for sample AE00316 analyzed on January 10, 2002.

NYC-WTC_000050963–000050976

Folder label: “GCMS X 1/7/02 A 1/9/02

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NYC 9/11 Public Portal Document Data File : C:\MSDCHEM\1\5973N\02JAN10\00316.D Vial: 3 Acq On : 10 Jan 2002 10:07 am Operator: Sample : 508 scan ext 1/7 Inst : Instrumen Mise : January 10, 2002 Multiplr: 1.00 MS Integration Params: SPLIT.P Quant Time: Jan 10 11:46:27 2002 Quant Results File: SCAN508.RES Quant Method : C:\MSDCHEM\1...\SCAN508.M (RTE Integrator) Title : 508 scan method Last Update : Thu Jan 10 11:01:02 2002 Response via : Initial Calibration DataAcq Meth : SCAN508

Compound R.T. Qlon Respons Cone Unit Qvalue 35) Di-n-butylphthalate 24.85 149 18305 0.07 ug/L 94 36) Fluoranthene 26.21 202 17872 0.09 ug/L 94 39) Pyrene 26.84 202 18046 0.07 ug/L # 83 40) Butylbenzylphthalate 0.00 149 0 N.D. 41) Benzo(a)anthracene 30.56 228 7558 0.04 ug/L 98 42) Bis(2-ethylhexyl)phthalate 31.11 149 54893 0.89 ug/L 95 43) Chrysene 30.50 228 14066 0.07 ug/L # 49 45) Di-n-octylphthalate 0.00 149 0 N.D. 46) Benzo(b)fluoranthene 0.00 252 0 N.D. \ 47) Benzo(k)fluoranthene 0.00 252 0 N.D. \ 48) Benzo(a)pyrene 34.40 252 9137 0.06 ug/L # 1 49) Indeno(1,2,3-cd)pyrene 0.00 276 0 N.D. \ 50) Dibenz(a,h)anthracene 0.00 278 0 N.D. \ 51) Benzo(g,h,i)perylene 0.00 276 0 N.D. \

(#) = qualifier out of range (m) = manual integration 00316.D SCAN508.M Thu Jan 10 11:46:27 2002 Page 2

NYC-WTC_000050966

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NYC-WTC_000050966Source: NYC Law Department, mirrored locally

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