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← Document results/DEP Box 28/GCMS X 1/7/02 A 1/9/02
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GCMS blank results for sample AE00277, Jan 2002

Machine-extracted title · confidence 90%

Blank analysis report for GCMS of sample AE00277 showing compounds below method detection limits from January 10, 2002.

NYC-WTC_000050825–000050837

Folder label: “GCMS X 1/7/02 A 1/9/02

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Scanned page image, NYC-WTC_000050832
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NYC 9/11 Public Portal Document Data File : C:\MSDCHEM\1\5973N\02JAN09\0107BLA.D Vial: 1 Acq On 9 Jan 2002 5:19 pm Operator: > Sample : lab blank 1/7 a Inst : Instrumen Mise : January 9, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\SCAN508.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 2 3,4-Dihydropyran $$ 2H-Pyra... Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T.

4.85 0.23 ug/L 93667 1,4-Dichlorobenzene-d4 9.71

Hit# Of 5 Tentative ID MW MolForm CAS# Qual

1 3,4-Dihydropyran $$ 2H-Pyran, 3,... 84 C5H80 000110-87-2 72 2 Furan, 2,3-dihydro-4-methyl- (CA... 84 C5H80 034314-83-5 64 3 2-METHYLBUT-2-ENAL 84 C5H80 000000-00-0 53 4 2-Butenal, 3-methyl-84 C5H80 000107-86-8 50 Abundance Scan 129 (4.847 min): 0107BLA.D (-) m/z 83.95 100.00% 84 __

55 5000 41 39 59

4.40 4.60 4.80 5.00 5.20

m/z-> 0 ' I ' ' ' ' I ' 30 35 .,.6,751., 40 45 50 55 60 65 I ■ ■ ' ' I ' ' ‘ ' I ' 1 1 ' I ' ’ 70 75 80 85 ' I ' 86 i 1 ■ ■ i ■ ■ ■ ■ i

90 95 m/z 55.00 55.07% Abundance #3375:3,4-Dihydropyran $$ 2H-Pyran, 3,4-dihydro- (CAS) $$... 55

y 84

5000 A I ' ' ' ' I ' ' ' i ' ■ 4.40 4.60 4.80 5.00 5.20 41 m/ z 41.10 40.09% 53 57 69 43 51 — ol • । • • ■ • । • ■ I 111 11 ■... | I ■ ' 11 1 1' i11 11 I rn/z--> 30 35 40 45 50 55 60 65 70 75 80 85 90 95 Abundance #3351: Furan, 2,3-dihydro-4-methyl- (CAS)$$ 4-METHYL-2,3-... 55 84 4.40 5000 3941 m/z

53 69 43 51 | 82 0 'I''''I'' I । ■ 1......... . 1 . . . I . . ‘ I‘ ■ I «■ । । 1 if ■n/z—> Abundance 30 35 40 45 50 55 60 65 #3298: 2-METHYLBUT-2-ENAL 55 70 75 80 85

84 90 95 ... .M.. 4.40 4 60 4.80 5.00 5.20 m/z 59.10 32.75% 5000

3941

m/z-> 0l ■ 30 i ■ ■ ■ ■ i ■ ■ 35 | 44 5153 i I । I ■ ■ I । ■ ■ ■ ■ | I । I I | I1111011119/0001101011111 ■ I ' ' 1 ' 1 1 1 ' 1 1 40 45 50 55> 60 65 70 75 80 85 90 95 4.40 AII 4.60 4.80 MA „A. 5.00 5.20

0107BLA.D SCAN508.M Thu Jan 10 11:51:32 2002 Page 4

NYC-WTC_000050832

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NYC-WTC_000050832Source: NYC Law Department, mirrored locally

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