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GCMS analysis results for sample AD31641, February 2002

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GCMS analysis report for sample AD31641 conducted on February 11, 2002.

NYC-WTC_000049745–000049761

Folder label: “GCMS X 1/2/02 A 1/3 - 1/4/02

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NYC 9/11 Public Portal Document

Library Search Compound Report Data File C: \HPCHEM\ 1 \DATA\JANO 302\31641.D Vial: 39 Acq On 4 Jan 2002 11:32 pm Operator: 209 GALOS Sample gems scan l/2a Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209.625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 9 Tetratetracontane Concentration Rank 6

R.T. EstConc Area Relative to ISTD R.T. 38.03 0.58 ug/1 61794 Perylene-dl2 36.90 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Tetratetracontane 619 C44H90 007098-22-8 86 2 Hexatriacontane 507 C36H74 000630-06-8 86 3 Tetradecane 198 C14H30 000629-59-4 86 4 Pentacosane 352 C25H52 _______ 000629-99-2 83 Abundance Scan 3593 (38.027 min): 31641.D (-) m/z 57.00 100.00% __ 57

5000 85

-WAlPA m/z-> 1.4416,37141, 200298 250 281300..................................... 50 100 150 350 400 450 500 550 600 37.60 37.80 38.00 38.20 38.40 m/z 43.00 61.98% Abundance #61068: Tetratetracontane 57

5000 85 T T T TT T 37.60 37.80 38.00 38.20 38.40 m/z 71.10 59.31% | | (113141 169 197 225 ITFtguimI"trh-iy r 379407 590618 miz-> 50l 100 150 200 250 300 350 400 450 500 550 6001 Abundance #59136: Hexatriacontane 57 Aaw0,A ./wAnA T 37.60 37.80 38.00 38.20 38.40 5000 85 m/z 85.05 47.88%

239 ...... 379407435 ,478506 ........... mfc-> 50 100 150 200 250 300 350 400 450 500 550 600 A AM A1i........... 1 "A AAA A Abundance #69659: Tetradecane | i i r r | > i r i |T 44/1 i 1'1 57 37.60 37.80 38.00 38.20 38.40 m/z 69.10 27.60% 5000 85

m/z—> u1 50 (13141168 ........................................... . 100 150 200 250 300 350 400 450 500 550 600 MAuALDMubauuk 37.60 37.80 38.00 38.20 38.40

31641.D GCMS1126.M Fri Feb 01 11:17:15 2002 Page 9 NYC-WTC_000049760

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NYC-WTC_000049760Source: NYC Law Department, mirrored locally

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