GCMS blank analysis results for sample AD31586, February 2002

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GCMS blank analysis report for sample AD31586 conducted on February 11, 2002.

NYC-WTC_000049693–000049702

Folder label: “GCMS X 1/2/02 A 1/3 - 1/4/02”

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NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed)

Data File C:\HPCHEM\l\DATA\JAN0302\31586.D Vial: 38 Acq On 4 Jan 2002 10:34 pm Operator: 209 GALOS Sample gems scan l/2a Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: RTEINT.P Quant Time: Feb 1 9:27 2002 Quant Results File: GCMS1126 .RES

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Tue Jan 22 11:56:23 2002 Response via : Initial Calibration DataAcq Meth : GCMS1126

Internal Standards R.T. Qlon Response Cone Units Dev(Min)

1) 1,4-Diehlorobenzene-d4 11.52 152 681539 20.00 ug/1 -0.18 10) Naphthalene-d8 15.12 136 2660133 20.00 ug/1 -0.18 17) Acenaphthene-diO 20.39 164 1316736 20.00 ug/1 -0.18 29) Phenanthrene-diO 24.81 188 1790632 20.00 ug/1 -0.18 38) Chrysene-dl2 32.83 240 975829 20.00 ug/1 -0.20 44) Perylene-dl2 36.90 264 567417 20.00 ug/1 -0.22

System Monitoring Compounds 37) 2,4-DDD 29.88 235 96871 4.92 ug/mL -0.19 Spiked Amount 5.000 Recovery = 98.40%

Target Compounds Qvalue 2) N-nitroso-dimethyl amine 0.00 74 0 N.D. 3) bis(2-Chloroethyl)ether 0.00 93 0 N.D. 4) 1,3-Dichlorobenzene 0.00 146 0 N.D. 5) 1,4-Dichlorobenzene 0.00 146 0 N.D. 6) 1,2-Dichlorobenzene 0.00 146 0 N.D. 7) 2,2' -oxybis(1-Chloropropan 0.00 45 0 N.D. 8) N-Nitroso-di-n-propylamine 0.00 70 0 N.D. 9) Hexachloroethane 0.00 117 0 N.D. 11) Nitrobenzene 0.00 77 0 N.D. 12) 1sophorone 0.00 82 0 N.D. 13) bis(2-Chloroethoxy)methane 0.00 93 0 N.D. 14) 1,2,4-Trichlorobenzene 0.00 180 0 N.D. 15) Naphthalene 15.19 128 542 N.D. 16) Hexachiorobutadiene 0.00 225 0 N.D. 18) Hexachiorocyclopentadiene 0.00 237 0 N.D. 19) 2-Chloronaphthalene 0.00 162 0 N.D. 20) Dimethylphthalate 0.00 163 0 N.D. 21) 2,6-Dinitrotoluene 0.00 165 0 N.D. 2 2) Acenaphthylene 0.00 152 0 N.D. 2 3) Acenaphthene 0.00 153 0 N.D. 24) 2,4-Dinitrotoluene 20.80 165 206 N.D. 25) Diethylphthalate 0.00 149 0 N.D. 26) 4-Chlorophenyl-phenylether 0.00 204 0 N.D. 27) Fluorene 0.00 166 0 N.D. 28) Azobenzen/ 1,2-Diphenylhyd 0.00 77 0 N.D.

(#) = qualifier out of range (m) = manual integration 31586.D GCMS1126.M Fri Feb 01 09:28:43 2002 Page 1

NYC-WTC_000049695

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