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GCMS results for sample AE09019, April 30, 2002

Machine-extracted title · confidence 100%

Laboratory report documenting GCMS analysis of sample AE09019 conducted on April 30, 2002.

NYC-WTC_000049431–000049440

Folder label: “GCMS X 4/16/02 A 4/26/02

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Scanned page image, NYC-WTC_000049436
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NYC 9/11 Public Portal Document LSC Area Percent Report Data File : C:\HPCHEM\l\DATA\APR2502\9019.D Vial: 23 Acq On : 25 Apr 2002 12:13 pm Operator: Sample : re-inject Inst : 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Method : C:\HPCHEM\1\METHODS\GCMS0412.M (RTE Integrator) Title : 209 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5 Signal : TIC

peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total 1 8.183 338 342 367 rBV 299995 737224 22.79% 4.585% 2 12.213 775 781 793 rBV 953703 2278387 70.43% 14.169% 3 14.811 1060 1064 1068 rBV2 26918 50966 1.58% 0.317% 4 15.839 1170 1176 1192 rBV 1378990 2889196 89.31% 17.968% 5 21.146 1748 1754 1771 rBV 1629020 3234893 100.00% 20.118% 6 23.285 1979 1987 1995 rVB 153872 296326 9.16% 1.843% 7 25.589 2231 2238 2249 rBV 1453060 3096325 95.72% 19.256% 8 33.640 3108 3115 3130 rBV 950985 2067401 63.91% 12.857% 9 37.863 3565 3575 3587 rBV2 471839 1428839 44.17% 8.886%

Sum of corrected areas: 16079557 9019.D GCMS0412.M Fri Apr 26 11:07:49 2002

NYC-WTC_000049436

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NYC-WTC_000049436Source: NYC Law Department, mirrored locally

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