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GCMS results for sample AE08971, April 30, 2002

Machine-extracted title · confidence 100%

Laboratory report documenting GCMS analysis of sample AE08971 conducted on April 30, 2002.

NYC-WTC_000049420–000049430

Folder label: “GCMS X 4/16/02 A 4/26/02

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Scanned page image, NYC-WTC_000049428
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OCR status: ok · source: pdftotext

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\APR2502\8971.D Vial: 17 Acq On : 26 Apr 2002 4:10 am Operator: Sample : re-inject Inst : 209 Misc Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0412.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 2 Cyclopentasiloxane, decamethyl Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T. --------------------------------------------------------------------- 14.80 2.14 ug/l 325788 Naphthalene-d8 15.84

Hit# of 5 1Tentative ID MW MolForm CAS# Qual

1 Cyclopenta 'loxane, decamethyl- -370 C10H3005Si5 000541-02-6~ 2 Benzeneeth namine, N-[(pentafluorop 475 C21H26F5NO2Si2 055429-85-1 37 .. 3 PhenethyJ. mine, N-methyl-.beta.,3,4 399 C18H37NO3Si3 010538-85-9 32 4 Benzoic cid, 2,4-bis[(trimethylsil 370 C16H3004Si3 010586-16-0 32 4bundance / Scan 1063 (14.805 min): 8971.D (-) m z 73 . 00 100 . 00%

267 355

14.80 108 133 154 177193 . r 1 .1 . r . ..-. . .'.... . ... 1Ye-1- 223 '1.' 293 323339 0 120 140 160 180 200 220 0 280 300 320 340 36 #51266: Cyclopentasi oxane, ethyl-

355 267

207 Ih 323339M

#74573: N-[(pentafluoroPheny4methylene1

m/z 356.05 14.141

151 179194 K;7 100 120 140 160 180 2( #74239: Phenethylamine, N-r 1 14.40 14.60 14.80 15.00 15.20 Im/z 268.00 10.18$

44 88 130147 193 KM ) 100 120 140 160 180 2C

8971.D GCMSO412.M Fri Apr 26 11:07:38 2002 Page 2

NYC-WTC 000049428

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NYC-WTC_000049428Source: NYC Law Department, mirrored locally

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