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GCMS results for sample AE08931, April 26, 2002

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Laboratory report documenting GCMS analysis of sample AE08931 conducted on April 26, 2002.

NYC-WTC_000049350–000049359

Folder label: “GCMS X 4/15/02 A 4/24/02

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NYC 9/11 Public Portal Document Quantitation Report (QT Reviewed) Data File : C:\HPCHEM\1\DATA\APR2302\8931.D Vial: 11 Acq On :24 Apr 2002 12:11 am Operator: Sample : gc/ms scan 4/15 Inst : 209 Mise : Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: Apr 24 8:20 2002 Quant Results File: GCMS0412.RES Quant Method : C:\HPCHEM\1\METHODS\GCMS0412.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Wed Apr 17 11:48:30 2002 Response via : Initial Calibration DataAcq Meth : GCMS0412

Compound R.T. Qlon Response Cone Unit Qvalue 3 3) Hexachlorobenzene 0.00 284 0 N.D. 3 4) Phenanthrene 25.58 178 343 N.D. 35) Anthracene 25.58 178 343 N.D. 36) Di-n-butylphthalate 27.55 149 3136 N.D. 3 7) Fluoranthene 0.00 202 0 N.D. 4 0) Pyrene 0.00 202 0 N.D. 41) Butylbenzylphthalate 0.00 149 0 N.D. 42) Benzo(a)anthracene 33.64 228 1786 N.D. 43) Bis(2-ethylhexyl)phthalate 33.86 149 875 N.D. 44) Chrysene 33.64 228 1786 N.D. 46) Di-n-Octylphthalate 36.06 149 488 N.D. 47) Benzo(b)fluoranthene 0.00 252 0 N.D. 48) Benzo(k)fluoranthene 0.00 252 0 N.D. 49) Benzo(a)pyrene 37.87 252 1649 N.D. 5 0) Indeno(1z 2,3-cd)pyrene 0.00 276 0 N.D. 51) Dibenz(a,h)anthracene 0.00 278 0 N.D. 52) Benzo(g,h,i)perylene 0.00 276 0 N.D.

(#) = qualifier out of range (m) = manual integration 8931.D GCMS0412.M Wed Apr 24 08:21:28 2002 Page 2

NYC-WTC_000049353

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NYC-WTC_000049353Source: NYC Law Department, mirrored locally

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