NYC 9/11 Public Portal Document
Quantitation Report (QT Reviewed)
. Data File : C:\MSDCHEM\1\DATA\042202\LBAA422.D Vial: 5
Acq On : 22 Apr 2002 2:22 pm Operator: Bohlk
Sample : LB 4/15/02 Inst : Instrumen
Mise : Multiplr: 1.00
MS Integration Params: BENZO.P
Quant Time: Apr 25 14:25:56 2002 Quant Results File: 5080402BBC.RES
Quant Method : C:\MSDCHEM\l\5973N\5080402BBC.M (RTE Integrator)
Title : Quantitation For Method 508gcscan
Last Update : Wed Apr 24 11:07:03 2002
Response via : Initial Calibration
DataAcq Meth : 508SCAN
Internal Standards R.T. Qlon Response Cone Units Dev(Min)
1) 1,4-Dichlorobenzene-d4 9.42 152 419441 40.00 ug/L 0.00
10) Naphthalene-d8 12.89 136 1967754 40.00 ug/L 0.00
17) Acenaphthene-diO 17.99 164 1149599 40.00 ug/L 0.00
30) Phenanthrene-diO 22.34 188 1585244 40.00 ug/L 0.00
39) Chrysene-dl2 30.14 240 1197814 40.00 ug/L -0.01
45) Perylene-dl2 34.02 264 697206 40.00 ug/L 0.00
System Monitoring Compounds
28) TCMX (SURR) 19.96 244 28683 6.25 ug/L 0.00
Spiked Amount 10.000 Recovery = 62.50%
38) 2,4-DDD (SURR) 0.00 235 0 0.00 ug/L
Spiked Amount 10.000 Recovery = 0.00%
Target Compounds Qvalue
2) N-nitroso-dimethyl amine 0.00 74 0 N.D.
3) bis(2-chloroethyl) ether 0.00 93 0 N.D.
4) 1,3 - Dichlorobenze 0.00 146 0 N.D.
5) 1,4 - Dichlorobenzene 0.00 146 0 N.D.
6) 1,2 - Dichlorobenzene 0.00 146 0 N.D.
7) 2,2 ‘ - oxybis (l-Chloropr 0.00 45 0 N.D.
8) N-Nitroso-di-n-propylamine 0.00 70 0 N.D.
9) Hexachloroethane 0.00 117 0 N.D.
11) Nitrobenzene 0.00 77 0 N.D.
12) Isophorone 0.00 82 0 N.D.
13) bis(2-Chloroethoxy) methan 0.00 93 0 N.D.
14) 1,2,4-Trichlorobenzene 0.00 180 0 N.D.
15) Naphthalene 0.00 128 0 N.D.
16) Hexachlorobutadiene 0.00 225 0 N.D.
18) Hexachlorocyclopentadiene 0.00 237 0 N.D.
19) 2-chloronaphthalene 0.00 162 0 N.D.
20) Dimethylphthalate 0.00 163 0 N.D.
21) 2,6-Dinitrotoluene 0.00 165 0 N.D. d
22) Acenaphthylene 0.00 152 0 N.D.
23) Acenaphthene 0.00 153 0 N.D.
24) 2,4-Dinitrotoluene 0.00 165 0 N.D.
25) Diethylphthalate 0.00 149 0 N.D.
26) 4-Chlorophenyl-phenyl ethe 0.00 204 0 N.D.
27) Fluorene 0.00 166 0 N.D.
29) Azobenzen/ 1,2-Diphenylhyd 0.00 77 0 N.D.
31) N-Nitrosodiphenylamine 0.00 169 0 N.D.
32) 4-Bromophenyl-phenyl ether 0.00 248 0 N.D.
3 3) Hexachlorobenzene 0.00 284 0 N.D.
34) Phenanthrene 0.00 178 0 N.D.
35) Anthracene 0.00 178 0 N.D.
36) Di-n-butylphthalate 0.00 149 0 N.D.
37) Fluoranthene 0.00 202 0 N.D.
40) .Pyrene 0.00 202 0 N.D.
41) Butylbenzylphthalate 0.00 149 0 N.D.
42) Benzo (a) antracene 0.00 228 0 N.D. d
43) Bis (2-ethylhexyl) phthala 0.00 149 0 N.D.
44) Chrysene 0.00 228 0 N.D. d
(#) = qualifier out of range (m) = manual integration
LBAA422.D 5080402BBC.M Thu Apr 25 14:26:58 2002 Page 1
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