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GCMS analysis results, sample AE08761, April 25, 2002

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Gas chromatography-mass spectrometry analysis of environmental sample AE08761, detecting unknown compounds and 2,4-DDD surrogate at 74 μg, completed April 25, 2002.

NYC-WTC_000049113–000049123

Folder label: “GCMS X 4/12/02 A 4/23/02

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NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed)

Data File : C:\HPCHEM\1\DATA\APR2 202\8761.D Vial: 23 Acq On : 23 Apr 2002 6:35 am Operator: Sample : gc/ms scan 4/12 Inst : 209 Mise Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: Apr 23 12:38 2002 Quant Results File: GCMS0412.RES Quant Method : C:\HPCHEM\1\METHODS\GCMS0412.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Wed Apr 17 11:48:30 2002 Response via : Initial Calibration DataAcq Meth : GCMS0412

Compound R.T. Qlon Response Cone Unit Qvalue 33) Hexachlorobenzene 0.00 284 0 N.D. 3 4) Phenanthrene 25.59 178 483 N.D. 3 5) Anthracene 25.59 178 483 N.D. 36) Di-n-butylphthalate 27.56 149 3930 N.D. 3 7) Fluoranthene 0.00 202 0 N.D. 4 0) Pyrene 0.00 202 0 N.D. 41) Butylbenzylphthalate 0.00 149 0 N.D. 4 2) Benzo(a)anthracene 33.64 228 2123 N.D. 43) Bis(2-ethylhexyl)phthalate 33.85 149 1178 N.D. 44) Chrysene 33.64 228 2123 N.D. 46) Di-n-Octylphthalate 36.06 149 1388 N.D. 47) Benzo(b)fluoranthene 0.00 252 0 N.D. 48) Benzo(k)fluoranthene 0.00 252 0 N.D. 4 9) Benzo(a)pyrene 37.88 252 2395 N.D. 50) Indeno(l,2,3-cd)pyrene 0.00 276 0 N.D. 51) Dibenz(a,h)anthracene 0.00 278 0 N.D. 52) Benzo(g,h,i)perylene 0.00 276 0 N.D.

(#) = qualifier out of range (m) = manual integration 8761.D GCMS0412.M Tue Apr 23 12:39:20 2002 Page 2

NYC-WTC_000049116

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NYC-WTC_000049116Source: NYC Law Department, mirrored locally

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