GCMS reference analysis results for sample AE08684, April 22, 2002

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8 Quantitation Report (QT Reviewed)

Data File : C:\HPCHEM\l\DATA\APR2202\REF2.D Vial: 5 Acq On : 22 Apr 2002 1:04 pm Operator: Sample : gc/ms scan 4/11 Inst : 209 Mise Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: Apr 22 14:53 2002 Quant Results File: GCMS0412.RES

Quant Method : C:\HPCHEM\1\METHODS\GCMS0412.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Wed Apr 17 11:48:30 2002 Response via : Initial Calibration DataAcq Meth : GCMS0412

Internal Standards R.T. Qlon Response Cone Units Dev(Min) 1) 1,4-Dichlorobenzene-d4 12.21 152 502735 20.00 ug/1 -0.03 10) Naphthalene-d8 15.85 136 1857720 20.00 ug/1 -0.03 17) Acenaphthene-diO 21.15 164 1061094 20.00 ug/1 -0.02 30) Phenanthrene-diO 25.59 188 1563017 20.00 ug/1 -0.03 39) Chrysene-dl2 33.65 240 1061389 20.00 ug/1 -0.03 45) Perylene-dl2 37.87 264 676933 20.00 ug/1 -0.05

System Monitoring Compounds 28) TCMX 23.29 209 47032 8.84 ug/L -0.04 Spiked Amount 10.000 Recovery = 88.40% 38) 2,4-DDD 0.00 235 0 0.00 ug/mL Spiked Amount 5.000 Recovery = 0.00% Target Compounds Qvalue 2) N-nitroso-dimethyl amine 5.87 74 100659 9.20 ug/1 99 3) bis(2-Chloroethyl)ether 11.61 93 250522 14.71 ug/1 98 4) 1,3-Dichlorobenzene 12.11 146 196882 11.21 ug/1 98 5) 1,4-Dichlorobenzene 12.26 146 207220 11.73 ug/1 99 6) 1,2-Dichlorobenzene 12.77 146 207227 12.63 ug/1 98 7) 2,2' -oxybis(1-Chloropropan 13.09 45 348152 14.80 ug/1 98 8) N-Nitroso-di-n-propylamine 13.48 70 160290 14.35 ug/1 99 9) Hexachloroethane 13.62 117 58292 9.00 ug/1 96 11) Nitrobenzene 13.89 77 228197 14.01 ug/1 99 12) 1sophorone 14.54 82 377878 12.26 ug/1 98 13) bis(2-Chloroethoxy)methane 15.22 93 300727 14.98 ug/1 99 14) 1,2,4-Trichlorobenzene 15.73 180 183112 12.97 ug/1 98 15) Naphthalene 15.90 128 660094 14.78 ug/1 100 16) Hexachlorobutadiene 16.45 225 61387 8.69 ug/1 99 18) Hexachlorocyclopentadiene 18.65 237 7247 1.54 ug/1 97 19) 2-Chloronaphthalene 19.41 162 401601 14.35 ug/1 97 20) Dimethylphthalate 20.49 163 531213 16.47 ug/1 98 21) 2,6-Dinitrotoluene 20.71 165 108613 14.08 ug/1 98 2 2) Acenaphthylene 20.67 152 585423 14.95 ug/1 99 23) Acenaphthene 21.24 153 426874 15.34 ug/1 99 24) 2,4-Dinitrotoluene 21.88 165 142195 14.00 ug/1 99 25) Diethylphthalate 22.63 149 503887 16.28 ug/1 98 26) 4-Chlorophenyl-phenylether 22.79 204 229944 16.75 ug/1 97 27) Fluorene 22.76 166 471534 16.00 ug/1 98 29) Azobenzen/ 1,2-Diphenylhyd 23.24 77 436792 13.34 ug/L 97 31) N-Nitrosodiphenylamine 23.17 168 149407 11.49 ug/1 98 32) 4-Bromophenyl-phenylether 24.25 248 129371 17.05 ug/1 97 (#) = qualifier out of range (m) = manual integration RER2 n CCMS0412 m Mon anr 20 1A.E5.11 anno Dace 1

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