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GCMS analysis results for sample AE05846, April 23, 2002

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GCMS laboratory report for sample AE05846 analyzed on April 23, 2002, by analyst DLV.

NYC-WTC_000048717–000048736

Folder label: “GCMS X 4/11/02 A 4/15/02

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NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed) Data File C:\HPCHEM\1\DATA\APRO 402\5846A.D Vial: 20 Acq On 4 Apr 2002 4:48 pm Operator: Sample gc/ms scan 3/12 Inst : GC/MS 209 Mise Multiplr: 2.00 MS Integration Params: GOOFY.P Quant Time: Apr 9 15:35 2002 Quant Results File: GCMS0408.RES Quant Method : C:\HPCHEM\1\METHODS\GCMS0408.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Mon Apr 08 11:30:53 2002 Response via : Initial Calibration DataAcq Meth : GCMS0403

Compound R.T. Qlon Response Cone Unit Qvalue 3 3) Hexachiorobenzene 0.00 284 0 N.D. 3 4) Phenanthrene 25.63 178 119 N.D. 35) Anthracene 0.00 178 0 N.D. 36) Di-n-butylphthalate 27.60 149 80584 4.24 ug/1 100 37) Fluoranthene 0.00 202 0 N.D. 4 0) Pyrene 0.00 202 0 N.D. 41) Butylbenzylphthalate 0.00 149 0 N.D. 4 2) Benzo(a)anthracene 33.68 228 950 N.D. 43) Bis(2-ethylhexyl)phthalate 33.90 149 3739 0.59 ug/1 # 94 44) Chrysene 33.68 228 950 N.D. 46) Di-n-Octylphthalate 0.00 149 0 N.D. 47) Benzo(b)fluoranthene 0.00 252 0 N.D. 48) Benzo(k)fluoranthene 0.00 252 0 N.D. 49) Benzo(a)pyrene 37.94 252 898 N.D. 50) Indeno(l,2,3-cd)pyrene 0.00 276 0 N.D. 51) Dibenz(a,h)anthracene 0.00 278 0 N.D. 52) Benzo(g,h,i)perylene 0.00 276 0 N.D.

(#) = qualifier out of range (m) = manual integration 5846A.D GCMS0408.M Tue Apr 16 08:04:40 2002 Page 2

NYC-WTC_000048729

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NYC-WTC_000048729Source: NYC Law Department, mirrored locally

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