GCMS analysis results for sample AE08425, May 2002

Machine-extracted title · confidence 100%

Laboratory report documenting GCMS analysis of sample AE08425 conducted on May 6, 2002, including surrogate recovery data.

NYC-WTC_000048148–000048168

Folder label: “GCMS X 4/9/02 A 4/19/02”

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NYC 9/11 Public Portal Document

LSC Area Percent Report

Data File : C:\MSDCHEM\l\DATA\020419\08425.D Vial: 12 Acq On : 19 Apr 2002 6:58 pm Operator: Nefliu Sample : sample Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: rteint.e

Method : C:\MSDCHEM\1\METHODS\SCAN020418.M (RTE Integrator) Title : Method 508 GC/MS Scan Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 5 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0.01 Peak Location: TOP

If leading or trailing edge 100 prefer < Baseline drop else tangent Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak corr. corr. % of # min scan scan scan TY height area % max. total 1 3.126 3 8 12 BV 2 42550 417677 0.52% 0.092% 2 5.006 317 328 342 PV 2 48284 947526 1.17% 0.210% 3 5.799 458 463 4 72 PV 2 30534 578910 0.72% 0.128% 4 6.105 509 515 532 PV 2 18774 509888 0.63% 0.113% 5 11.375 1398 1412 1434 PV 1935843 51399972 63.63% 11.370%

6 16.534 2274 2290 2313 PV 2643409 70979800 87.86% 15.702% 7 16.763 2322 2329 2338 W 2 7075 202728 0.25% 0.045% 8 24.460 3614 3639 3655 PV 2858854 80785148 100.00% 17.871% 9 27.539 4151 4163 4175 PV 3 253409 6995634 8.66% 1.548% 10 31.094 4753 4768 4777 W 4 20052 639852 0.79% 0.142%

11 31.722 4852 4875 4890 BV 2 2627443 80105239 99.16% 17.720% 12 31.957 4905 4915 4929 W 2 25899 764271 0.95% 0.169% 13 34.807 5393 5400 5409 PV 2 15116 351108 0.43% 0.078% 14 36.423 5667 5675 5682 PV 5 15579 387203 0.48% 0.086% 15 36.611 5687 5707 5716 W 3 8100 335176 0.41% 0.074%

16 37.210 5801 5809 5812 PV 3 6525 129915 0.16% 0.029% 17 37.639 5876 5882 5889 W 3 9055 241198 0.30% 0.053% 18 38.544 6028 6036 6052 W 1444025 27374758 33.89% 6.056% 19 38.650 6052 6054 6061 W 2 16259 438032 0.54% 0.097% 20 39.220 6142 6151 6159 W 4 19151 647331 0.80% 0.143%

21 39.472 6189 6194 6198 W 3 13387 297872 0.37% 0.066% 22 39.937 6261 6273 6288 W 2 3527749 68970088 85.37% 15.257% 23 40.301 6326 6335 6343 W 6 12808 484484 0.60% 0.107% 24 40.436 6350 6358 6364 W 3 21148 563459 0.70% 0.125% 25 40.524 6367 6373 6378 W 5 16869 402736 0.50% 0.089%

26 41.100 6463 6471 6473 W 3 7204 142756 0.18% 0.032% 27 41.364 6506 6516 6525 PV 5 16224 391048 0.48% 0.087% 28 43.156 6807 6821 6839 PV 2 2809659 56571021 70.03% 12.514%

Sum of corrected areas: 452054831

08425.D SCAN020418.M Thu May 02 15:28:00 2002 Page 1

NYC-WTC_000048152

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NYC-WTC_000048152Source: NYC Law Department, mirrored locally

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