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GCMS analysis results for sample AE08425, May 2002

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Laboratory report documenting GCMS analysis of sample AE08425 conducted on May 6, 2002, including surrogate recovery data.

NYC-WTC_000048148–000048168

Folder label: “GCMS X 4/9/02 A 4/19/02

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NYC 9/11 Public Portal Document Tentatively Identified Compound (LSC) summary . Operator ID: Nefliu Date Acquired: 19 Apr 2002 6:58 pm Data File: C:\MSDCHEM\1\DATA\020419\08425.D Name: sample Mise: Method: C:\MSDCHEM\1\METHODS\SCAN020418.M (Chemstation Integrator) Title: Method 508 GC/MS Scan Library Searched: C:\DATABASE\nist98.1

--Internal Standard-- TIC Top Hit name RT EstConc Units Response # RT Resp Cone

Heptane 3.12 0.3 ug/1 417677 1 11.37 51400000 40.0 VButenol, methyl- 5.00 0.7 ug/1 947526 1 11.37 51400000 40.0 3-Penten-2-ol 5.80 0.5 ug/1 578910 1 11.37 51400000 40.0 . 3 Pentanol-;—3-met. . 6.10 0.4 ug/1 509888 1 11.37 51400000 40.0 Thiouyanic acid, . . . 31.09 0.3 ug/1 639852 4 31.72 80105200 40.0 Anthracene-d10 - P&ucfaur34?96 Azetidine, 1 - me t hy l - 36.42 0.4 ug/1 0.2 ug/1 764271 387203 4 31.72 80105200 40.0 5 39.93 68970100 40.0 1-Heneicosyl formate 38.55 15.9 ug/1 27374800 5 39.93 68970100 40.0 .—)—cis--Myrtanyla.. . 38.65 0.3 ug/1 438032 5 39.93 68970100 40.0 p-Terphenyl-dl4 39.22 0.4 ug/1 647331 5 39.93 68970100 40.0 2—Pentanol,—5—(2-- . . . 40.30 0.3 ug/1 484484 5 39.93 68970100 40.0 Benzoic acid;—p-a. . . 40.44 0.3 ug/1 563459 5 39.93 68970100 40.0 Bis (2 ethylhexyl) . . . 40.52 0.2 ug/1 402736 5 39.93 68970100 40.0 Propanoic acid,—3- .. 41.37 0.2 ug/1 391048 5 39.93 68970100 40.0

08425.D SCAN020418.M Thu May 02 15:28:13 2002 Page 17

NYC-WTC_000048168

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NYC-WTC_000048168Source: NYC Law Department, mirrored locally

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