GCMS analysis report for sample AE08212 showing surrogate recovery and unknown compounds from April 2002.
NYC-WTC_000048027–000048037Folder label: “GCMS X 4/8/02 A 4/18/02”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document
Library Search Compound Report
Data File : C:\HPCHEM\l\DATA\APR1702\8212.D Vial: 23 Acq On : 18 Apr 2002 5:42 am Operator: Sample : gc/ms scan 4/8 Inst : 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS0412.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L
Peak Number 3 Benzoic acid, 2,4-bis[(trimeth Concentration Rank 2
R.T. EstConc Area Relative to ISTD R.T.
40.49 0.50 ug/1 41533 Perylene-dl2 37.87
Hit# of 5 Tentative ID MW MolForm CAS# Qual
1 Benzoic acid/ 2,4-bis[(trimethylsil 370 C16H30O4Si3 010586-16-0 22 2 Cyclopentasiloxane, decamethyl- 370 C10H3005Si5 000541-02-6 10 3 Benzoic acid, 2,5-bis(trimethylsilo 370 C16H3004Si3 003618-20-0 10 4 N-Methyladrenaline, tri-TMS 413 C19H39NO3Si3 000000-00-0 10 Abundance Scan 3861 (40.488 min): 8212. D (-) m/z 73.00 100.00% 73 __ 147 221 5000 355 281 44 96 429 253 327 40.20 40.40 40.60 40.80 " i11" ।।" 1 .................. 1 i" " r " i" " i" " r HI i 'r " ‘ i" " i1'" i" ‘ ‘ i ‘ ‘‘I’ " P H' r " ■ i 1 m/z 147.00 62.03%
_A_ m/z-> 40 60 80 100120140160180200220240260280300 320340360380 400420 Abundance #73975: Benzoic acid, 2,4-bis[(trimethylsilyl)oxy]-, trimet 73
5000 355 40.20 40.40 40.60 40.80 45 m/Z 221.05 55.82% 133 193 223 281 i''111111 ri" "r "'i ‘'r',,‘ ■ r1"ir 111 ।\।। ।।. I" " I'" ■ I''111 ■'" I /z-> 40 60 80 100120140160180200220240260280300 320340360380400420 Abundance #51266: Cyclopentasiloxane, decamethyl- 73
355 40.20 40.40 40.60 40.80 267 m/z 355.05 42.89% 5000
207 249 323 , TTTUg l" " (" " 1 "'l" '"l"'11" " I'"' " I n/z-> 40 60 80 100120140160180200220240260280300 320 340360380400420 — Abundance #73978: Benzoic acid, 2,5-bis(trimethylsiloxy)-, trimethyls 73 40.20 40.40 40.60 40.80 355 m/z 281.00 30.47% / 5000
45
| 1 " 11 " " | " 1 ' | ,147 | | 179 223, 267 297 | । 1 11 i i ! ' p 1 iV| ! ! । 11 TTri > i r| i i i i 11 i i i । i i ‘ T i ■ " 11r 1111 m/z—> 40 60 80 100120140160180200220240260280300320340360380400420 40.20 40.40 40.60 40.80
8212 .D GCMS0412,M Thu Apr 18 14:12:12 2002 Page 3
NYC-WTC_000048036
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Ranked by indexed similarity. Reasons describe shared subjects and filing context; check the source records.
NYC-WTC_000049113
Gas chromatography-mass spectrometry analysis of environmental sample AE08761, detecting unknown compounds and 2,4-DDD surrogate at 74 μg, completed April 25, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000049370
Laboratory report documenting GCMS analysis of sample AE08933 conducted on April 26, 2002.
1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000049350
Laboratory report documenting GCMS analysis of sample AE08931 conducted on April 26, 2002.
1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000049360
Laboratory report documenting GCMS analysis of sample AE08932 conducted on April 26, 2002.
1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000049167
Laboratory report documenting GCMS analysis of sample AE08836 conducted on April 25, 2002, showing detection of unknown compounds.
1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000048069
GCMS analysis report for sample AE08216 showing surrogate recovery and unknown compounds from April 2002.
1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000049330
Laboratory report documenting GCMS analysis of sample AE08839 conducted on April 26, 2002.
1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000048846
GCMS laboratory report for sample AE08681 analyzed on April 23, 2002, by analyst DLV.
1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000060522
DEP laboratory report of GCMS analysis for sample AE06756 conducted on April 18, 2002.
1 shared non-person entities · 1 shared topics · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000058627
Instrument data for GCMS method 508 scan including internal standards from March 4, 2002.
1 shared topics · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000005322
Laboratory report documenting GCMS analysis of sample AE02602 conducted on March 7, 2002, including surrogate recovery data.
1 shared topics · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000010176
Laboratory report documenting GCMS analysis of sample AE01650 conducted on March 4, 2002, including surrogate recovery data.
1 shared topics · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗Similar subjects in other documents. Similarity does not establish the same event, measurement or conclusion.
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NYC-WTC_000047951
Department of Environmental Protection GCMS analysis record dated April 8-18, 2002.
Filed in the same folder
NYC-WTC_000047952
Laboratory log sheet for Method 20 recording parameters and sample processing details from April 2002.
Filed in the same folder
NYC-WTC_000047955
GCMS blank analysis report for sample AE08209 listing volatile organic compounds from April 2002.
Filed in the same folder
NYC-WTC_000047967
GCMS calibration results for volatile organic compounds from sample AE08209 analyzed in April 2002.
Filed in the same folder
NYC-WTC_000047971
GCMS reference analysis report for volatile organic compounds from sample AE08209 analyzed in April 2002.
Filed in the same folder