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GCMS analysis results, sample AE08210, April 2002

Machine-extracted title · confidence 80%

Gas chromatography-mass spectrometry analysis of sample AE08210 detecting unknown organic compounds and measuring 2,4-DDD surrogate recovery at 73%, April 22, 2002.

NYC-WTC_000048013–000048026

Folder label: “GCMS X 4/8/02 A 4/18/02

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NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed)

Data File C:\HPCHEM\1\DATA\APR17 02\8 210.D Vial: 21 Acq On 18 Apr 2002 3:45 am Operator: Sample gc/ms scan 4/8 Inst : 209 Mise Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: Apr 18 14:03 2002 Quant Results File: GCMS0412.RES Quant Method : C:\HPCHEM\1\METHODS\GCMS0412.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Wed Apr 17 11:48:30 2002 Response via : Initial Calibration DataAcq Meth : GCMS0412

Compound R.T. Qlon Response Cone Unit Qvalue 33) Hexachlorobenzene 0.00 284 0 N.D. 3 4) Phenanthrene 25.59 178 416 N.D. 35) Anthracene 25.59 178 416 N.D. 36) Di-n-butylphthalate 27.56 149 1491 N.D. 37) Fluoranthene 0.00 202 0 N.D. 40) Pyrene 0.00 202 0 N.D. 41) Butylbenzylphthalate 0.00 149 0 N.D. 42) Benzo(a)anthracene 33.64 228 2138 N.D. 43) Bis(2-ethylhexyl)phthalate 33.86 149 1323 N.D. 44) Chrysene 33.64 228 2789 N.D. 46) Di-n-Octylphthalate 35.59 149 285 N.D. 47) Benzo(b)fluoranthene 36.69 252 561 N.D. 48) Benzo(k)fluoranthene 36.75 252 517 N.D. 49) Benzo(a)pyrene 37.88 252 2114 N.D. 50) Indeno(1,2,3-cd)pyrene 0.00 276 0 N.D. 51) Dibenz(a,h)anthracene 0.00 278 0 N.D. 52) Benzo(g,h,i)perylene 43.18 276 362 N.D.

(#) = qualifier out of range (m) = manual integration 8210 .D GCMS0412.M Thu Apr 18 14:04:18 2002 Page 2

NYC-WTC_000048016

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NYC-WTC_000048016Source: NYC Law Department, mirrored locally

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