GCMS results sample AE08211, April 2002

NYC 9/11 Public Portal Document

LSC Area Percent Report

Data File : C:\HPCHEM\1\DATA\APR1702\8211.D Vial: 22 Acq On : 18 Apr 2002 4:44 am Operator: Sample : gc/ms scan 4/8 Inst : 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\HPCHEM\1\METHODS\GCMS0412.M (RTE Integrator) Title : 209 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total

1 12.212 775 781 793 rBV 938630 2286650 71.70% 15.098% 2 15.847 1171 1177 1191 rBV 1378293 2873350 90.09% 18.972% 3 21.144 1748 1754 1769 rBV 1600429 3189247 100.00% 21.057% 4 23.283 1980 1987 1994 rVB 142824 279336 8.76% 1.844% 5 25.587 2231 2238 2249 rBV 1460807 3027485 94.93% 19.989%

6 33.638 3108 3115 3121 rBV2 932150 2040450 63.98% 13.472% 7 33.703 3121 3122 3132 rW 28761 40357 1.27% 0.266% 8 37.871 3568 3576 3597 rBV2 488319 1408576 44.17% 9.300%

Sum of corrected areas: 15145451

8211.D GCMS0412 .M Thu Apr 18 14:11:51 2002

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