GCMS blank analysis AE08209, April 2002

NYC 9/11 Public Portal Document

LSC Area Percent Report

Data File : C:\HPCHEM\l\DATA\APR1702\LBA.D Vial: 16 Acq On : 17 Apr 2002 10:52 pm Operator: Sample : gc/ms scan 4/8 Inst : 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\HPCHEM\1\METHODS\GCMS0412.M (RTE Integrator) Title : 209 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge <100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total

1 12.210 775 780 802 rBV 956111 2384856 70.09% 14.903% 2 15.846 1170 1176 1193 rBV 1493421 3031627 89.10% 18.945% 3 21.143 1747 1753 1771 rBV 1620645 3402391 100.00% 21.262% 4 23.282 1979 1986 1992 rBV 142156 275777 8.11% 1.723% 5 25.586 2230 2237 2249 rBV2 1477866 3079771 90.52% 19.246% 6 33.637 3107 3114 3133 rBV2 893056 1984392 58.32% 12.401% 7 37.309 3508 3514 3525 rVB3 21597 72755 2.14% 0.455% 8 37.869 3567 3575 3594 rBV 507874 1503675 44.19% 9.397% 9 38.750 3661 3671 3679 rBV3 21878 82348 2.42% 0.515% 10 40.495 3850 3861 3870 rBV7 17355 80169 2.36% 0.501% 11 42.661 4086 4097 4103 rBV6 12041 61735 1.81% 0.386% 12 45.397 4385 4395 4404 rVB4 7269 42677 1.25% 0.267%

Sum of corrected areas: 16002173 LBA.D GCMS0412.M Thu Apr 18 14:13:45 2002

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