GCMS analysis results for sample AE08253, April 2002

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•88 30.882 4717 4732 4773 W 2 2354703 54366197 85.39% 15.386% 89 31.153 4773 4778 4781 W 4 6735 153346 0.24% 0.043% 90 31.182 4781 4783 4785 W 4754 58623 0.09% 0.017%

91 31.206 4785 4787 4789 W 4386 52677 0.08% 0.015% 92 31.229 4789 4791 4794 W 2 4175 53539 0.08% 0.015% 93 31.458 4823 4830 4848 W 5 9563 443654 0.70% 0.126% 94 32.122 4939 4943 4951 W 2 3081 72473 0.11% 0.021% 95 32.610 5018 5026 5029 W 2142 52126 0.08% 0.015%

96 32.874 5061 5071 5075 W 2 2284 63103 0.10% 0.018% 97 33.333 5140 5149 5154 W 6 3473 92407 0.15% 0.026% 98 33.432 5162 5166 5171 W 4 2268 42543 0.07% 0.012% 99 33.556 5185 5187 5191 W 3 2625 39477 0.06% 0.011% 100 34.096 5277 5279 5283 W 2 1764 22875 0.04% 0.006%

101 34.314 5314 5316 5318 W 1871 18663 0.03% 0.005% 102 34.449 5333 5339 5345 W 4 4695 124633 0.20% 0.035% 103 34.572 5356 5360 5363 W 2048 36036 0.06% 0.010% 104 34.790 5380 5397 5435 W 2 1750626 43676422 68.60% 12.361% 105 35.025 5435 5437 5439 W 3 6998 87402 0.14% 0.025%

106 35.048 5439 5441 5443 W 2 6171 68078 0.11% 0.019% 107 35.072 5443 5445 5460 W 5 5387 264812 0.42% 0.075% 108 35.219 5466 5470 5479 W 5 3850 130135 0.20% 0.037% 109 35.354 5492 5493 5504 W 6 3624 105328 0.17% 0.030% 110 35.512 5508 5520 5526 W 5 7672 270391 0.42% 0.077%

ill 36.082 5613 5617 5626 W 3 3083 108835 0.17% 0.031% 112 36.182 5632 5634 5638 W 3574 55000 0.09% 0.016% 113 36.423 5672 5675 5679 W 3 2844 51676 0.08% 0.015% 114 36.605 5696 5706 5716 W 5 6789 285385 0.45% 0.081% 115 36.682 5716 5719 5731 W 2 3476 159483 0.25% 0.045%

116 36.881 5751 5753 5757 W 3 3738 54024 0.08% 0.015% 117 36.946 5760 5764 5766 W 2 3276 55579 0.09% 0.016% 118 37.075 5784 5786 5795 W 4 3132 91632 0.14% 0.026% 119 37.158 5795 5800 5804 W 5 2915 77657 0.12% 0.022% 120 37.205 5804 5808 5812 W 2 3444 75939 0.12% 0.021%

121 37.727 5892 5897 5899 W 2 2917 51989 0.08% 0.015% 122 37.892 5921 5925 5927 W 3 3783 49830 0.08% 0.014% 123 37.921 5927 5930 5939 W 4 5708 152316 0.24% 0.043% 124 38.021 5945 5947 5956 W 3 2923 88744 0.14% 0.025% 125 38.127 5963 5965 5967 W 2883 26781 0.04% 0.008%

126 38.474 6018 6024 6029 W 4 2608 59455 0.09% 0.017% 127 38.515 6029 6031 6037 W 4 2598 61446 0.10% 0.017% 128 38.668 6055 6057 6061 W 3295 48159 0.08% 0.014% 129 38.844 6084 6087 6090 W 2 2396 31624 0.05% 0.009% 130 39.226 6150 6152 6158 W 4 1872 35089 0.06% 0.010%

131 39.273 6158 6160 6162 W 2 2128 19621 0.03% 0.006% 132 39.296 6162 6164 6168 W 3 2149 32220 0.05% 0.009% 133 39.508 6192 6200 6202 W 4 2963 70660 0.11% 0.020% 134 39.525 6202 6203 6217 W 6 3428 102957 0.16% 0.029% 135 39.643 6221 6223 6229 W 2 2250 38588 0.06% 0.011%

136 39.831 6250 6255 6257 PV 2 1232 16959 0.03% 0.005%

08253.D 041702SCAN.M Fri Apr 19 08:37:55 2002 Page 3

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