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GCMS analysis results for sample AE08014, April 2002

Machine-extracted title · confidence 100%

Laboratory report documenting GCMS analysis of sample AE08014 conducted on April 24, 2002, including surrogate recovery data.

NYC-WTC_000047682–000047690

Folder label: “GCMS X 4/4/02 A 4/12/02

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Scanned page image, NYC-WTC_000047687
OCR text

OCR status: ok · source: pdftotext

NYC 9/11 Public Portal Document

LSC Area Percent Report

Data File : C:\HPCHEM\l\DATA\APR1102\8014.D Vial: 20 Acq On : 12 Apr 2002 9:03 am Operator: Sample : gc/ms scan 4/4 Inst : 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\HPCHEM\1\METHODS\GCMS0412.M (RTE Integrator) Title : 209 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total

1 12.231 777 783 799 rVB 1041806 2385791 68.78% 14.472% 2 14.829 1060 1066 1072 rBV 32586 64706 1.87% 0.393% 3 15.857 1172 1178 1196 rBV 1392394 3055549 88.08% 18.535% 4 21.163 1750 1756 1769 rBV 1682026 3468875 100.00% 21.043% 5 23.302 1980 1989 1997 rVB 170192 342862 9.88% 2.080%

6 25.606 2233 2240 2251 rBV2 1580555 3326500 95.90% 20.179% 7 27.571 2450 2454 2461 rVB 50172 96173 2.77% 0.583% 8 33.658 3111 3117 3131 rBV2 917995 2176044 62.73% 13.200% 9 37.899 3571 3579 3599 rBV2 502088 1568532 45.22% 9.515%

Sum of corrected areas: 16485032

8014.D GCMS0412.M Tue Apr 16 12:07:22 2002

NYC-WTC_000047687

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NYC-WTC_000047687Source: NYC Law Department, mirrored locally

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