GCMS analysis results for sample AE07976, April 18, 2002

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Laboratory report documenting GCMS analysis of sample AE07976 conducted on April 18, 2002.

NYC-WTC_000047593–000047607

Folder label: “GCMS X 4/4/02 A 4/15/02”

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NYC 9/11 Public Portal Document

LSC Area Percent Report

Data File : C:\MSDCHEM\l\DATA\020415\07976.D Vial: 16 Acq On : 15 Apr 2002 11:05 pm Operator: Nefliu Sample : sample Inst : Instrumen Mise : Multiplr: 1.00 MS Integration Params: LSCINT.e

Method : C:\MSDCHEM\1\METHODS\041202SCAN.M (Chemstation Integrator) Title : 508 Modified GC/MS scan

Signal : TIC

peak R.T. first max last PK peak corr. corr. % of # min scan scan scan TY height area % max. total

1 3.144 4 11 21 BV 5 7150 165372 0.33% 0.064% 2 3.385 47 52 57 PV 9516 146536 0.30% 0.057% 3 3.667 95 100 106 PV 15919 249702 0.51% 0.096% 4 3.708 106 107 109 W 2 2276 21757 0.04% 0.008% 5 3.755 109 115 118 W 6 3141 72688 0.15% 0.028%

6 3.796 118 122 129 W 2 6365 149442 0.30% 0.058% 7 4.213 190 193 197 W 5 2025 36841 0.07% 0.014% 8 4.313 197 210 216 W 6 2307 77949 0.16% 0.030% 9 4.401 216 225 228 PV 4 1723 30656 0.06% 0.012% 10 4.807 288 294 297 W 6 1998 39116 0.08% 0.015%

11 4.889 302 308 316 W 5 2933 76339 0.15% 0.029% 12 4.995 320 326 332 W 5 2657 53919 0.11% 0.021% 13 5.147 347 352 369 W 6 9002 200884 0.41% 0.078% 14 5.970 485 492 4 98 PV 21962 389109 0.79% 0.150% 15 6.035 498 503 513 W 2 42573 850365 1.72% 0.328%

16 7.492 745 751 761 PV 3 2872 57740 0.12% 0.022% 17 8.855 972 983 992 BV 3 2803 60329 0.12% 0.023% 18 9.642 1105 1117 1126 W 4 1944 60384 0.12% 0.023% 19 9.783 1137 1141 1144 PV 3 164 5 25938 0.05% 0.010% 20 9.989 1166 1176 1196 W 1819360 31337106 63.48% 12.097%

21 10.306 1211 1230 1236 W 5 2817 118103 0.24% 0.046% 22 11.910 1498 1503 1508 W 4 3043 51113 0.10% 0.020% 23 12.081 1525 1532 1537 W 2 2816 51444 0.10% 0.020% 24 12.574 1611 1616 1624 W 4 1854 32379 0.07% 0.012% 25 12.762 1645 1648 1654 PV 2 1670 20390 0.04% 0.008%

26 13.485 1748 1771 1784 BV 2385207 41723138 84.52% 16.106% 27 13.638 1792 1797 1813 W 6252 133258 0.27% 0.051% 28 13.767 1813 1819 1822 W 2 2266 35070 0.07% 0.014% 29 13.879 1827 1838 1843 PV 3 6434 94614 0.19% 0.037% 30 16.799 2327 2335 2344 PV 4 3231 62359 0.13% 0.024%

31 18.632 2632 2647 2662 PV 2657981 49366183 100.00% 19.057% 32 19.020 2708 2713 2720 W 4 2518 59579 0.12% 0.023% 33 20.600 2969 2982 2989 PV 238181 4199805 8.51% 1.621% 34 21.828 3187 3191 3195 W 3 1673 29207 0.06% 0.011% 35 22.645 3322 3330 3337 W 2 14217 267278 0.54% 0.103%

36 23.021 3383 3394 3414 W 2 2575459 49287350 99.84% 19.026% 37 23.174 3414 3420 3430 W 20555 538303 1.09% 0.208%

07976.D 041202SCAN.M Tue Apr 16 13:46:01 2002 Page 1

NYC-WTC_000047597

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NYC-WTC_000047597Source: NYC Law Department, mirrored locally

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