GCMS analysis results for sample AE07974, April 18, 2002

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Laboratory report documenting GCMS analysis of sample AE07974 conducted on April 18, 2002.

NYC-WTC_000047564–000047576

Folder label: “GCMS X 4/4/02 A 4/15/02”

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NYC 9/11 Public Portal Document

LSC Area Percent Report

Data File : C:\MSDCHEM\l\DATA\020415\07974 .D Vial: 14 Acq On : 15 Apr 2002 9:26 pm Operator: Nefliu Sample : sample Inst Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e

Method : C:\MSDCHEM\1\METHODS\041202SCAN.M (Chemstation Integrator) Title : 508 Modified GC/MS scan

Signal : TIC

peak R.T. first max last PK peak corr. corr. % of # min scan scan scan TY height area % max. total

1 3.115 3 6 9 BV 4 3522 38078 0.07% 0.014% 2 3.156 9 13 23 PV 5 3013 60503 0.12% 0.022% 3 3.350 44 46 52 W 4 2313 33171 0.07% 0.012% 4 3.637 91 95 100 PV 3 3205 54153 0.11% 0.020% 5 3.714 100 108 111 W 2 3031 80240 0.16% 0.029%

6 3.773 ill 118 124 W 4 6713 212887 0.42% 0.078% 7 3.837 124 129 133 W 5 3918 115899 0.23% 0.042% 8 3.884 133 137 144 W 7 3835 118179 0.23% 0.043% 9 4.789 286 291 295 W 5 2691 58055 0.11% 0.021% 10 4.836 295 299 304 W 5 2639 56634 0.11% 0.021%

11 4.889 304 308 317 W 7 3433 102392 0.20% 0.037% 12 4.977 321 323 329 W 2 4193 68376 0.13% 0.025% 13 5.136 345 350 361 W 8 5676 156551 0.31% 0.057% 14 5.665 435 440 443 W 5 2424 40156 0.08% 0.015% 15 5.964 485 491 4 96 PV 18407 334365 0.66% 0.122%

16 6.017 496 500 519 W 44856 963858 1.90% 0.351% 17 8.156 861 864 867 W 2 1720 18300 0.04% 0.007% 18 9.384 1064 1073 1076 PV 4 1105 26767 0.05% 0.010% 19 9.989 1167 1176 1192 PV 1846528 31866712 62.73% 11.619% 20 10.300 1226 1229 1242 W 3 2245 53570 0.11% 0.020%

21 12.081 1529 1532 1537 W 3 1692 22823 0.04% 0.008% 22 13.485 1739 1771 1790 PV 2424386 42459302 83.58% 15.482% 23 13.638 1790 1797 1803 PV 2 4754 86784 0.17% 0.032% 24 14.307 1907 1911 1919 W 5 1999 30062 0.06% 0.011% 25 15.759 2145 2158 2162 PV 5 1933 40568 0.08% 0.015%

26 16.799 2331 2335 2340 PV 3500 49564 0.10% 0.018% 27 18.632 2637 2647 2674 PV 2736489 49952371 98.33% 18.214% 28 19.020 2709 2713 2718 W 4 1853 31443 0.06% 0.011% 29 20.207 2911 2915 2920 PV 3 1948 28797 0.06% 0.011% 30 20.600 2973 2982 2992 W 223529 3939231 7.75% 1.436%

31 22.645 3320 3330 3342 W 15040 279095 0.55% 0.102% 32 23.021 3382 3394 3414 PV 2 2541544 50800838 100.00% 18.523% 33 23.174 3414 3420 3432 W 19495 467457 0.92% 0.170% 34 23.256 3432 3434 3442 W 4 1515 24888 0.05% 0.009% 35 25.160 3751 3758 3771 W 40379 745843 1.47% 0.272%

36 27.240 4107 4112 4118 W 2 1791 23919 0.05% 0.009% 37 30.888 4719 4733 4772 PV 2 2357725 49424736 97.29% 18.021%

07974.D 041202SCAN.M Tue Apr 16 13:44:34 2002 Page 1

NYC-WTC_000047568

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NYC-WTC_000047568Source: NYC Law Department, mirrored locally

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NYC-WTC_000046841

Laboratory report documenting GCMS analysis of sample AE08069 including surrogate recovery and unknown compounds on April 18, 2002.

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