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GCMS method file details for April 3-5, 2002

Machine-extracted title · confidence 90%

Technical documentation listing GC/MS method parameters and internal standard data for analysis performed in early April 2002.

NYC-WTC_000047452–000047462

Folder label: “GCMS X 4/3/02 A 4/5/02

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Scanned page image, NYC-WTC_000047456
OCR text

OCR status: ok · source: pdftotext

NYC 9/11 Public Portal Document

LSC Area Percent Report

Data File C:\MSDCHEM\l\DATA\020404\07767.D Vial: 21 Acq On 5 Apr 2002 1:34 am Operator: Nefliu Sample sample Inst Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e

Method : C:\MSDCHEM\1\METHODS\SCAN020403.M (Chemstation Integrator) Title : Method 508 GC/MS Scan

Signal : TIC

peak R.T. first max last PK peak corr. corr. % of # min scan scan scan TY height area % max. total

1 3.273 22 33 37 PV 3 3649 120527 0.53% 0.106% 2 3.314 37 40 48 W 2 5815 120453 0.53% 0.106% 3 3.367 48 49 54 W 2 2021 37415 0.16% 0.033% 4 3.420 54 58 62 W 4 1732 30820 0.14% 0.027% 5 5.594 419 428 441 PV 3 5527 167050 0.74% 0.146%

6 10.659 1280 1290 1309 W 543921 13849627 61.00% 12.137% 7 15.770 2147 2160 2171 PV 761340 18337941 80.77% 16.071% 8 23.655 3489 3502 3517 W 853261 21811807 96.07% 19.115% 9 26.728 4014 4025 4034 W 142949 3478902 15.32% 3.049% 10 30.254 4614 4625 4626 BV 2 2138 29505 0.13% 0.026%

11 30.271 4626 4628 4637 W 2 2421 42650 0.19% 0.037% 12 30.900 4717 4735 4747 W 2 798874 22704701 100.00% 19.898% 13 31.135 4759 4775 4781 W 2 2582 70722 0.31% 0.062% 14 33.979 5243 5259 5271 BV 7274 150759 0.66% 0.132% 15 39.096 6118 6130 6149 PV 2 1137077 20400449 89.85% 17.878%

16 42.299 6665 6675 6700 PV 694441 12754626 56.18% 11.178%

Sum of corrected areas: 114107954

07767.D SCAN020403 .M Fri Apr 05 14:31:47 2002 Page 1

NYC-WTC_000047456

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NYC-WTC_000047456Source: NYC Law Department, mirrored locally

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