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GCMS analysis results, sample AE07519, April 2002

Machine-extracted title · confidence 100%

Gas chromatography-mass spectrometry analysis of sample AE07519 performed on April 11, 2002, showing unknown compounds and 2,4-DDD surrogate at 98 ug with 5.0 ug MDL.

NYC-WTC_000047413–000047422

Folder label: “GCMS X 4/2/02 A 4/4/02

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NYC 9/11 Public Portal Document

LSC Area Percent Report

Data File C:\MSDCHEM\1\DATA\020404\07519.D Vial: 15 Acq On 4 Apr 2002 8:00 pm Operator: Nefliu Sample sample Inst Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e

Method : C:\MSDCHEM\1\METHODS\SCAN020403.M (Chemstation Integrator) Title : Method 508 GC/MS Scan

Signal : TIC

peak R.T. first max last PK peak corr. corr. % of # min scan scan scan TY height area % max. total

1 3.308 22 39 43 PV 4 4752 167829 0.73% 0.148% 2 3.343 43 45 50 VB 4 1477 19923 0.09% 0.018% 3 5.041 329 334 341 PB 3 1972 35865 0.16% 0.032% 4 5.588 422 427 434 PV 2 5082 93334 0.41% 0.082% 5 10.658 1277 1290 1311 PV 537512 13890859 60.72% 12.225%

6 15.770 2144 2160 2174 PV 757698 18353061 80.22% 16.152% 7 23.661 3489 3503 3520 W 849164 21917965 95.80% 19.289% 8 26.722 4014 4024 4041 PV 2 66170 1477084 6.46% 1.300% 9 30.271 4615 4628 4641 W 2 2492 85154 0.37% 0.075% 10 30.894 4720 4734 4747 W 2 808025 22878442 100.00% 20.134%

11 31.123 4760 4773 4782 PV 2 2429 79864 0.35% 0.070% 12 39.096 6107 6130 6161 PV 2 1162073 20817321 90.99% 18.320% 13 39.443 6185 6189 6197 W 2 2882 49456 0.22% 0.044% 14 42.298 6656 6675 6701 PV 2 720559 13582349 59.37% 11.953% 15 43.009 6791 6796 6807 W 3 2805 57828 0.25% 0.051%

16 43.826 6928 6935 6941 PV 4 2662 68461 0.30% 0.060% 17 44.778 7088 7097 7104 PV 3 2254 54119 0.24% 0.048%

Sum of corrected areas: 113628914

07519.D SCAN020403.M Fri Apr 05 14:29:49 2002 Page 1

NYC-WTC_000047417

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NYC-WTC_000047417Source: NYC Law Department, mirrored locally

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